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22 BAB 3 SPESIFIKASI ALAT Tabel 3.1 Spesifikasi Heater 1A & 1B SPESIFIKASI ALAT Nama Alat Heater Kode Alat Fungsi Memanaskan Udara Sebelum Masuk Reaktor Jenis

Shell and tube heat exchanger Tube Side Fluida Udara Laju alir fluida 564806,6267 (lb/jam) Temperatur masuk 87,8 (F) Temperatur keluar 177,8 (F) 12708149,1 329,521 940,620

Shell Side Fluida Steam Laju alir fluida 10008,94 (lb/jam) Temperatur masuk 464 (F) Temperatur keluar 464 (F) Kalor umpan, Qumpan (BTU/hr) ∆T LMTD Koreksi (oF) Luas perpindahan panas (A), ft2 Clean overall coefficient, Uc (Btu/(hr)(ft2)(oF) Design overall coefficient, UD (Btu/(hr)(ft2)(oF)

8,550 40,738 Allowable 0,02

Dirt factor, RD (hr)(ft2)(oF)/Btu Shell Side Shell ID (in) 25 Baffle Space, B (in) 4 Passes 2 Clearance, C’ (in) 0,25 Equivalent 0,0825 diameter, de

Corrected 0,0092 Tube Side

Tube OD (in) Tube ID (in) Number of tube, Nt Tube length, L (ft)

1 0,810 226 16

BWG Flow area /tube, a’ (in) Pitch (square) Passes

Pressure Drop, ∆P (psi)

H-01A & 1B

Allowab le

Calculat ed

3

0,218

Pressure Drop, ∆P (psi)

13 0,515 1,25 6 Allowab Calculat le ed 3

0,37

Pra-Rancangan Pabrik Maleic Anhydride dari Butana Kel. VII/S. Genap/2018 Oleh

Diperiksa

1. Jufri Suanto Sitinjak

1. Jufri Suanto Sitinjak 2. Lamria Eufransia 3. Samuel Nainggolan

2. Lamria Eufransia 3. Samuel Nainggolan

Disetujui

23

GAMBAR ALAT

T in

t out

T out

t in

Gambar 3.1 2-6 Heat Exchanger (kern,1965)

Tabel 3.2 Spesifikasi Heater 2 Pra-Rancangan Pabrik Maleic Anhydride dari Butana Kel. VII/S. Genap/2018 Oleh

Diperiksa

1. Jufri Suanto Sitinjak

1. Jufri Suanto Sitinjak 2. Lamria Eufransia 3. Samuel Nainggolan

2. Lamria Eufransia 3. Samuel Nainggolan

Disetujui

24 SPESIFIKASI ALAT Heater Kode Alat H-02 Memanaskan LPG Butana Sebelum Masuk Reaktor

Nama Alat Fungsi Jenis

Shell and tube heat exchanger Tube Side Fluida Butana Laju alir fluida 8382,991 (lb/jam) Temperatur masuk 77 (F) Temperatur keluar 302 (F) 880505,026 253,492 77,189

Shell Side Steam

Fluida Laju alir fluida 693,486 (lb/jam) Temperatur masuk 464 (F) Temperatur keluar 464 (F) Kalor umpan, Qumpan (BTU/hr) ∆T LMTD Koreksi (oF) Luas perpindahan panas (A), ft2 Clean overall coefficient, Uc (Btu/(hr)(ft2)(oF) Design overall coefficient, UD (Btu/(hr)(ft2)(oF) 2

27,891 42,535 Allowable 0,02

o

Dirt factor, RD (hr)(ft )( F)/Btu Shell Side Shell ID (in) 10 Baffle Space, B (in) 4 Passes 2 Clearance, C’ (in) 0,25 Equivalent 0,0825 diameter, de

Corrected 0,012 Tube Side

Tube OD (in) Tube ID (in) Number of tube, Nt Tube length, L (ft) BWG Flow area /tube, a’ (in) Pitch (square) Passes

Pressure Drop, ∆P (psi)

1 0,675 26 16

Allowab le

Calculat ed

3

0,001

Pressure Drop, ∆P (psi)

13 0,515 1,25 4 Allowab Calculat le ed 3

0,004

Pra-Rancangan Pabrik Maleic Anhydride dari Butana Kel. VII/S. Genap/2018 Oleh

Diperiksa

1. Jufri Suanto Sitinjak

1. Jufri Suanto Sitinjak 2. Lamria Eufransia 3. Samuel Nainggolan

2. Lamria Eufransia 3. Samuel Nainggolan

Disetujui

25 GAMBAR ALAT

T in

t out

T out

t in

Gambar 3.2 2-4 Heat Exchanger (kern,1965)

Tabel 3.3 Spesifikasi Heater 3 SPESIFIKASI ALAT Pra-Rancangan Pabrik Maleic Anhydride dari Butana Kel. VII/S. Genap/2018 Oleh

Diperiksa

1. Jufri Suanto Sitinjak

1. Jufri Suanto Sitinjak 2. Lamria Eufransia 3. Samuel Nainggolan

2. Lamria Eufransia 3. Samuel Nainggolan

Disetujui

26 Nama Alat

Heater Kode Alat H-02 Memanaskan LPG Butana dan Udara Sebelum Masuk Reaktor

Fungsi Jenis

Shell and tube heat exchanger Tube Side Fluida Udara + Butana Laju alir fluida 1137995,142 (lb/jam) Temperatur masuk 566,6 (F) Temperatur keluar 734 (F) 50353256,61 365,741 1122,598

Shell Side Steam

Fluida Laju alir fluida 32604,315 (lb/jam) Temperatur masuk 1022 (F) Temperatur keluar 1022 (F) Kalor umpan, Qumpan (BTU/hr) ∆T LMTD Koreksi (oF) Luas perpindahan panas (A), ft2 Clean overall coefficient, Uc (Btu/(hr)(ft2)(oF) Design overall coefficient, UD (Btu/(hr)(ft2)(oF) 2

95,739 122,639 Allowable 0,02

o

Dirt factor, RD (hr)(ft )( F)/Btu Shell Side Shell ID (in) 27 Baffle Space, B (in) 4 Passes 2 Clearance, C’ (in) 0,25 Equivalent 0,083 diameter, de

Tube Side Tube OD (in) Tube ID (in) Number of tube, Nt Tube length, L (ft) BWG Flow area /tube, a’ (in) Pitch (square) Passes

Pressure Drop, ∆P (psi)

Corrected 0,002

Allowab le

Calculat ed

3

2,158

Pressure Drop, ∆P (psi)

1 0,810 268 16 13 0,515

1,25 4 Allowab Calculat le ed 3

0,047

GAMBAR ALAT Pra-Rancangan Pabrik Maleic Anhydride dari Butana Kel. VII/S. Genap/2018 Oleh

Diperiksa

1. Jufri Suanto Sitinjak

1. Jufri Suanto Sitinjak 2. Lamria Eufransia 3. Samuel Nainggolan

2. Lamria Eufransia 3. Samuel Nainggolan

Disetujui

27

T in

t out

T out

t in

Gambar 3.3 2-4 Heat Exchanger (kern,1965)

Tabel 3.4 Spesifikasi Cooler 1A & 1B SPESIFIKASI ALAT Nama Alat Cooler Kode Alat

C-01A & 01B

Pra-Rancangan Pabrik Maleic Anhydride dari Butana Kel. VII/S. Genap/2018 Oleh

Diperiksa

1. Jufri Suanto Sitinjak

1. Jufri Suanto Sitinjak 2. Lamria Eufransia 3. Samuel Nainggolan

2. Lamria Eufransia 3. Samuel Nainggolan

Disetujui

28 Fungsi

Mendinginkan Produk Reaktor Sebelum Masuk Absorber

Jenis

Shell and tube heat exchanger Tube Side Fluida MA dan Udara Laju alir fluida 568997,5709 (lb/jam) Temperatur masuk 464 (F) Temperatur keluar 230 (F) 33286357,9 198,334 427,258

Shell Side Air Pendingin

Fluida Laju alir fluida 264177,4436 (lb/jam) Temperatur masuk 77 (F) Temperatur keluar 203 (F) Kalor umpan, Qumpan (BTU/hr) ∆T LMTD Koreksi (oF) Luas perpindahan panas (A), ft2 Clean overall coefficient, Uc (Btu/(hr)(ft2)(oF) Design overall coefficient, UD (Btu/(hr)(ft2)(oF) 2

89,797 384,834 Allowable 0,02

o

Dirt factor, RD (hr)(ft )( F)/Btu Shell Side Shell ID (in) 27 Baffle Space, B (in) 4 Passes 2 Clearance, C’ (in) 0,375 Equivalent 0,123 diameter, de

Tube Side Tube OD (in) Tube ID (in) Number of tube, Nt Tube length, L (ft) BWG Flow area /tube, a’ (in) Pitch (square) Passes

Pressure Drop, ∆P (psi)

Corrected 0,01

Allowab le

Calculat ed

10

7,987

Pressure Drop, ∆P (psi)

1,5 1,31 102 16 13 1,350

1,875 4 Allowab Calculat le ed 10

0,116

GAMBAR ALAT

Pra-Rancangan Pabrik Maleic Anhydride dari Butana Kel. VII/S. Genap/2018 Oleh

Diperiksa

1. Jufri Suanto Sitinjak

1. Jufri Suanto Sitinjak 2. Lamria Eufransia 3. Samuel Nainggolan

2. Lamria Eufransia 3. Samuel Nainggolan

Disetujui

29

T in

t out

T out

t in

Gambar 3.4 2-4 Heat Exchanger (kern,1965)

Tabel 3.5 Spesifikasi Cooler 2 SPESIFIKASI ALAT Nama Alat Cooler Kode Alat C-02 Fungsi Mendinginkan Suhu Dibutil Ftalat Sebelum Masuk Absorber Pra-Rancangan Pabrik Maleic Anhydride dari Butana Kel. VII/S. Genap/2018 Oleh

Diperiksa

1. Jufri Suanto Sitinjak

1. Jufri Suanto Sitinjak 2. Lamria Eufransia 3. Samuel Nainggolan

2. Lamria Eufransia 3. Samuel Nainggolan

Disetujui

30 Jenis

Shell and tube heat exchanger Tube Side Fluida Dibutil Ftalat Laju alir fluida 17400,559 (lb/jam) Temperatur masuk 325 (F) Temperatur keluar 86 (F) 1877769,358 51,068 213,574

Shell Side Air Pendingin

Fluida Laju alir fluida 20864,10397 (lb/jam) Temperatur masuk 77 (F) Temperatur keluar 167 (F) Kalor umpan, Qumpan (BTU/hr) ∆T LMTD Koreksi (oF) Luas perpindahan panas (A), ft2 Clean overall coefficient, Uc (Btu/(hr)(ft2)(oF) Design overall coefficient, UD (Btu/(hr)(ft2)(oF) 2

167,405 168,721 Allowable 0,02

o

Dirt factor, RD (hr)(ft )( F)/Btu Shell Side Shell ID (in) 15,25 Baffle Space, B (in) 4 Passes 2 Clearance, C’ (in) 0,25 Equivalent 0,083 diameter, de

Corrected 0,000 Tube Side

Tube OD (in) Tube ID (in) Number of tube, Nt Tube length, L (ft) BWG Flow area /tube, a’ (in) Pitch (square) Passes

Pressure Drop, ∆P (psi)

1 0,810 68 16

Allowab le

Calculat ed

10

0,531

Pressure Drop, ∆P (psi)

13 0,515 1,25 4 Allowab Calculat le ed 10

0,004

GAMBAR ALAT

Pra-Rancangan Pabrik Maleic Anhydride dari Butana Kel. VII/S. Genap/2018 Oleh

Diperiksa

1. Jufri Suanto Sitinjak

1. Jufri Suanto Sitinjak 2. Lamria Eufransia 3. Samuel Nainggolan

2. Lamria Eufransia 3. Samuel Nainggolan

Disetujui

31 T in

t out

T out

t in

Gambar 3.5 2-4 Heat Exchanger (kern,1965)

Tabel 3.6 Spesifikasi Cooler 3 SPESIFIKASI ALAT Nama Alat Cooler Kode Alat C-03 Fungsi Menurunkan Suhu Maleic Anhydride Sebelum Masuk Tangki Jenis

Shell and tube heat exchanger

Pra-Rancangan Pabrik Maleic Anhydride dari Butana Kel. VII/S. Genap/2018 Oleh

Diperiksa

1. Jufri Suanto Sitinjak

1. Jufri Suanto Sitinjak 2. Lamria Eufransia 3. Samuel Nainggolan

2. Lamria Eufransia 3. Samuel Nainggolan

Disetujui

32 Shell Side Air Pendingin

Tube Side Dibutil Ftalat

Fluida Laju alir fluida 5217,252 (lb/jam) Temperatur masuk 77 (F) Temperatur keluar 167 (F) Kalor umpan, Qumpan (BTU/hr) ∆T LMTD Koreksi (oF) Luas perpindahan panas (A), ft2 Clean overall coefficient, Uc (Btu/(hr)(ft2)(oF) Design overall coefficient, UD (Btu/(hr)(ft2)(oF) 2

Fluida Laju alir fluida 6960,215 (lb/jam) Temperatur masuk 339,8 (F) Temperatur keluar 176 (F) 469552,7335 129,641 62,816 40,975 56,356 Allowable 0,02

o

Dirt factor, RD (hr)(ft )( F)/Btu Shell Side Shell ID (in) 8 Baffle Space, B (in) 4 Passes 2 Clearance, C’ (in) 0,25 Equivalent 0,079 diameter, de

Tube Side Tube OD (in) Tube ID (in) Number of tube, Nt Tube length, L (ft) BWG Flow area /tube, a’ (in) Pitch (square) Passes

Pressure Drop, ∆P (psi)

Corrected 0,007

Allowab le

Calculat ed

10

0,023

Pressure Drop, ∆P (psi)

0,75 0,56 20 16 13 0,247

1 4 Allowab Calculat le ed 10

0,004

GAMBAR ALAT

Pra-Rancangan Pabrik Maleic Anhydride dari Butana Kel. VII/S. Genap/2018 Oleh

Diperiksa

1. Jufri Suanto Sitinjak

1. Jufri Suanto Sitinjak 2. Lamria Eufransia 3. Samuel Nainggolan

2. Lamria Eufransia 3. Samuel Nainggolan

Disetujui

33 T in

t out

T out

t in

Gambar 3.6 2-4 Heat Exchanger (kern,1965)

Tabel 3.7 Spesifikasi Heat Exchanger 1A & 1B SPESIFIKASI ALAT Nama Alat Heat Exchanger Kode Alat HE-01A & 01B Menukar Panas Umpan Reaktor dengan Produk Keluaran Fungsi Reaktor Pra-Rancangan Pabrik Maleic Anhydride dari Butana Kel. VII/S. Genap/2018 Oleh

Diperiksa

1. Jufri Suanto Sitinjak

1. Jufri Suanto Sitinjak 2. Lamria Eufransia 3. Samuel Nainggolan

2. Lamria Eufransia 3. Samuel Nainggolan

Disetujui

34 Jenis

Shell and tube heat exchanger Tube Side Fluida Udara + Butana Laju alir fluida 568998,1222 (lb/jam) Temperatur masuk 287,6 (K) Temperatur keluar 555,8 (K) 36681599,58 177,498 1004,800

Shell Side Udara + MA

Fluida Laju alir fluida 568997,5709 (lb/jam) Temperatur masuk 734 (K) Temperatur keluar 464 (K) Kalor umpan, Qumpan (BTU/hr) ∆T LMTD Koreksi (oF) Luas perpindahan panas (A), ft2 Clean overall coefficient, Uc (Btu/(hr)(ft2)(oF) Design overall coefficient, UD (Btu/(hr)(ft2)(oF) 2

27,221 205,672 Allowable 0,02

o

Dirt factor, RD (hr)(ft )( F)/Btu Shell Side Shell ID (in) 33 Baffle Space, B (in) 4 Passes 2 Clearance, C’ (in) 0,375 Equivalent 0,123 diameter, de

Corrected 0,032 Tube Side

Tube OD (in) Tube ID (in) Number of tube, Nt Tube length, L (ft) BWG Flow area /tube, a’ (in) Pitch (square) Passes

Pressure Drop, ∆P (psi)

1,5 1,31 160 16

Allowab le

Calculat ed

10

4,267

Pressure Drop, ∆P (psi)

13 1,35 1,875 6 Allowab Calculat le ed 10

0,001

GAMBAR ALAT

Pra-Rancangan Pabrik Maleic Anhydride dari Butana Kel. VII/S. Genap/2018 Oleh

Diperiksa

1. Jufri Suanto Sitinjak

1. Jufri Suanto Sitinjak 2. Lamria Eufransia 3. Samuel Nainggolan

2. Lamria Eufransia 3. Samuel Nainggolan

Disetujui

35 T in

t out

T out

t in

Gambar 3.7 2-6 Heat Exchanger (kern,1965)

Tabel 3.8 Spesifikasi Heat Exchanger 2 SPESIFIKASI ALAT Nama Alat Heat Exchanger Kode Alat HE-02 Fungsi Pertukaran Panas Umpan Distilasi dan Keluaran Reboiler Pra-Rancangan Pabrik Maleic Anhydride dari Butana Kel. VII/S. Genap/2018 Oleh

Diperiksa

1. Jufri Suanto Sitinjak

1. Jufri Suanto Sitinjak 2. Lamria Eufransia 3. Samuel Nainggolan

2. Lamria Eufransia 3. Samuel Nainggolan

Disetujui

36 Jenis Shell Side Dbutil Ftalat + MA

Fluida Laju alir fluida 24360,4872 (lb/jam) Temperatur masuk 203 (F) Temperatur keluar 441,05 (F) Kalor umpan, Qumpan (BTU/hr) ∆T LMTD Koreksi (oF) Luas perpindahan panas (A), ft2 Clean overall coefficient, Uc (Btu/(hr)(ft2)(oF) Design overall coefficient, UD (Btu/(hr)(ft2)(oF) 2

Shell and tube heat exchanger Tube Side Fluida Dibutil Ftalat Laju alir fluida 17400,559 (lb/jam) Temperatur masuk 637,89 (F) Temperatur keluar 364,1 (F) 2632752,346 141,081 364,333 25,570 46,098 Allowable 0,02

o

Dirt factor, RD (hr)(ft )( F)/Btu Shell Side Shell ID (in) 15,25 Baffle Space, B (in) 4 Passes 2 Clearance, C’ (in) 0,25 Equivalent 0,079 diameter, de

Corrected 0,02 Tube Side

Tube OD (in) Tube ID (in) Number of tube, Nt Tube length, L (ft) BWG Flow area /tube, a’ (in) Pitch (square) Passes

Pressure Drop, ∆P (psi)

0,75 0,56 116 16

Allowab le

Calculat ed

10

1,543

Pressure Drop, ∆P (psi)

13 0,247 1 4 Allowab Calculat le ed 10

0,0016

GAMBAR ALAT

Pra-Rancangan Pabrik Maleic Anhydride dari Butana Kel. VII/S. Genap/2018 Oleh

Diperiksa

1. Jufri Suanto Sitinjak

1. Jufri Suanto Sitinjak 2. Lamria Eufransia 3. Samuel Nainggolan

2. Lamria Eufransia 3. Samuel Nainggolan

Disetujui

37 T in

t out

T out

t in

Gambar 3.8 2-4 Heat Exchanger (kern,1965)

Tabel 3.9 Spesifikasi Condensor 1 SPESIFIKASI ALAT Nama Alat Condensor Kode Alat CD-01 Fungsi Merubah Fasa dan Mendinginkan Produk Top Distilasi 1 Jenis

Shell and tube heat exchanger

Pra-Rancangan Pabrik Maleic Anhydride dari Butana Kel. VII/S. Genap/2018 Oleh

Diperiksa

1. Jufri Suanto Sitinjak

1. Jufri Suanto Sitinjak 2. Lamria Eufransia 3. Samuel Nainggolan

2. Lamria Eufransia 3. Samuel Nainggolan

Disetujui

38 Shell Side Maleic Anhydride

Tube Side Air Pendingin

Fluida Laju alir fluida 6960,303 (lb/jam) Temperatur masuk 402,47 (F) Temperatur keluar 339,8 (F) Kalor umpan, Qumpan (BTU/hr) ∆T LMTD Koreksi (oF) Luas perpindahan panas (A), ft2 Clean overall coefficient, Uc (Btu/(hr)(ft2)(oF) Design overall coefficient, UD (Btu/(hr)(ft2)(oF) 2

Fluida Laju alir fluida 5914,986 (lb/jam) Temperatur masuk 77 (F) Temperatur keluar 158 (F) 479113,8491 43,63 113,069 123,297 15,975 Allowable 0,02

o

Dirt factor, RD (hr)(ft )( F)/Btu Shell Side Shell ID (in) 10 Baffle Space, B (in) 4 Passes 2 Clearance, C’ (in) 0,25 Equivalent 0,079 diameter, de

Tube Side Tube OD (in) Tube ID (in) Number of tube, Nt Tube length, L (ft) BWG Flow area /tube, a’ (in) Pitch (square) Passes

Pressure Drop, ∆P (psi)

Corrected 0,0054

Allowab le

Calculat ed

10

9,073

Pressure Drop, ∆P (psi)

0,75 0,56 36 16 13 0,247

1 4 Allowab Calculat le ed 10

2,053

GAMBAR ALAT

Pra-Rancangan Pabrik Maleic Anhydride dari Butana Kel. VII/S. Genap/2018 Oleh

Diperiksa

1. Jufri Suanto Sitinjak

1. Jufri Suanto Sitinjak 2. Lamria Eufransia 3. Samuel Nainggolan

2. Lamria Eufransia 3. Samuel Nainggolan

Disetujui

39 T in

t out

T out

t in

Gambar 3.9 2-4 Heat Exchanger (kern,1965)

Tabel 3.10 Spesifikasi Reboiler 1 SPESIFIKASI ALAT Nama Alat Heat Exchanger Kode Alat RB-01 Fungsi Merubah Fasa Maleic Anhydride pada Kolom Distilasi Jenis

Shell and tube heat exchanger

Pra-Rancangan Pabrik Maleic Anhydride dari Butana Kel. VII/S. Genap/2018 Oleh

Diperiksa

1. Jufri Suanto Sitinjak

1. Jufri Suanto Sitinjak 2. Lamria Eufransia 3. Samuel Nainggolan

2. Lamria Eufransia 3. Samuel Nainggolan

Disetujui

40 Shell Side Dbutil Ftalat + MA

Fluida Laju alir fluida 24360,4872 (lb/jam) Temperatur masuk 440,6 (F) Temperatur keluar 636,98 (F) Kalor umpan, Qumpan (BTU/hr) ∆T LMTD Koreksi (oF) Luas perpindahan panas (A), ft2 Clean overall coefficient, Uc (Btu/(hr)(ft2)(oF) Design overall coefficient, UD (Btu/(hr)(ft2)(oF) 2

Tube Side Steam

Fluida Laju alir fluida 4498,894 (lb/jam) Temperatur masuk 734 (F) Temperatur keluar 734 (F) 3758376,636 177,658 163,3216 32,968 129,529 Allowable 0,02

o

Dirt factor, RD (hr)(ft )( F)/Btu Shell Side Shell ID (in) 12 Baffle Space, B (in) 4 Passes 1 Clearance, C’ (in) 0,25 Equivalent 0,079 diameter, de

Tube Side Tube OD (in) Tube ID (in) Number of tube, Nt Tube length, L (ft) BWG Flow area /tube, a’ (in) Pitch (square) Passes

Pressure Drop, ∆P (psi)

Corrected 0,022

Allowab le

Calculat ed

10

neg

Pressure Drop, ∆P (psi)

0,75 0,56 52 16 13 0,247

1 2 Allowab Calculat le ed 10

neg

GAMBAR ALAT

Pra-Rancangan Pabrik Maleic Anhydride dari Butana Kel. VII/S. Genap/2018 Oleh

Diperiksa

1. Jufri Suanto Sitinjak

1. Jufri Suanto Sitinjak 2. Lamria Eufransia 3. Samuel Nainggolan

2. Lamria Eufransia 3. Samuel Nainggolan

Disetujui

41 t out

T in

t in

T out

Gambar 3.10 1-2 Heat Exchanger (Reboiler) (kern,1965)

Pra-Rancangan Pabrik Maleic Anhydride dari Butana Kel. VII/S. Genap/2018 Oleh

Diperiksa

1. Jufri Suanto Sitinjak

1. Jufri Suanto Sitinjak 2. Lamria Eufransia 3. Samuel Nainggolan

2. Lamria Eufransia 3. Samuel Nainggolan

Disetujui

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