Standar Akrilamid_10.pdf

Sample Information Analyzed by : SOFIA NOFIANTI Analyzed : 1/1/2019 10:23:36 PM Sample Type : Standar Akrilamida 10 ppm Level # :1 Sample Name : Pembanding Sample ID : Akrilamida 10 ppm IS Amount : [1]=1.000 Sample Amount : 1.000 Dilution Factor : 1.000 Vial # :1 Injection Volume : 1.000 Data File : C:\GCMSsolution\Sample\Penelitian Mahasiswa\Kopi\Standar Akrilamid_10.QGD Org Data File : C:\GCMSsolution\Sample\Penelitian Mahasiswa\Kopi\Standar Akrilamid_10.QGD Method File : C:\GCMSsolution\METODA ANALYSIS\Akrilamid_meth.qgm Org Method File : C:\GCMSsolution\METODA ANALYSIS\Akrilamid_meth.qgm Report File : C:\GCMSsolution\Data\Omega3_6\Report.QGR Tuning File : C:\GCMSsolution\System\Tune1\Tuning 2019\Januari\Tgl 2.qgt [Comment] Kode sampel Standar Akrilamid 10 ppm Modified by : SOFIA NOFIANTI Modified : 1/1/2019 10:54:15 PM

Peak# 1 2 3 4 5 6 7 8 9 10 11 12 13 14

R.Time 2.021 2.674 2.750 2.792 2.842 2.942 16.146 16.367 16.590 16.773 17.381 17.558 17.660 17.940

AreaArea% 788756 34.44 111925 4.89 64413 2.81 31717 1.38 20440 0.89 12170 0.53 17465 0.76 28808 1.26 10220 0.45 42073 1.84 10076 0.44 20682 0.90 22305 0.97 427135 18.65

20.0

46

44 45

41 42 43

31

32 34 33 35 36 37 38 39 40

11 12 13

7 8 910

10.0

14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30

TIC

432 6 5

intensity 1,000,000

30.0

Peak Report TIC Height Height% Name Base m/z 155387 34.05 Methanol (CAS) Carbinol 31.00 23251 5.09 Benzo[g]pteridine-2,4(3H,10H)-dione, 8-hydroxy-7,10-dimethyl- (CAS) 8-HYDROXY-7,10-DIMETH 32.00 15697 3.44 97.15 12016 2.63 77.05 7690 1.69 44.00 2308 0.51 39.05 8777 1.92 74.10 2016 0.44 56.05 4402 0.96 98.15 14839 3.25 91.10 3668 0.80 129.15 4496 0.99 129.15 6013 1.32 207.00 53101 11.64 69.10

Peak# 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46

R.Time 18.342 18.731 18.783 18.833 18.950 19.042 19.100 19.200 19.342 19.417 19.511 19.600 19.662 20.164 20.243 20.317 20.864 22.093 22.350 22.459 22.558 22.850 23.002 23.125 23.292 23.602 26.308 26.708 26.742 27.514 27.601 29.917

AreaArea% 12151 0.53 20668 0.90 17026 0.74 21555 0.94 62960 2.75 29963 1.31 22094 0.96 68437 2.99 18520 0.81 27586 1.20 36963 1.61 13666 0.60 12489 0.55 39607 1.73 22908 1.00 11395 0.50 11824 0.52 14453 0.63 14544 0.64 11048 0.48 11401 0.50 12529 0.55 14928 0.65 27347 1.19 11049 0.48 10758 0.47 23187 1.01 15143 0.66 15787 0.69 22357 0.98 12163 0.53 15553 0.68 2290244100.00

Height Height% Name 1851 0.41 5300 1.16 6552 1.44 5505 1.21 8447 1.85 8360 1.83 7545 1.65 7542 1.65 5929 1.30 6041 1.32 7555 1.66 4254 0.93 3363 0.74 7054 1.55 5327 1.17 4053 0.89 2040 0.45 4126 0.90 2602 0.57 4315 0.95 2583 0.57 2210 0.48 6875 1.51 4123 0.90 2668 0.58 1671 0.37 2480 0.54 2843 0.62 1171 0.26 2652 0.58 3158 0.69 2496 0.55 456352100.00

Base m/z 56.05 147.15 95.15 85.15 54.05 147.15 147.15 41.10 79.10 79.10 79.10 55.05 61.05 61.05 61.05 61.05 111.15 54.05 70.10 84.10 95.15 95.15 82.15 95.15 42.10 40.00 40.00 96.10 96.10 40.00 42.10 40.00