Probation Period Report.ppt

Probation Period Report By Miranti Puspitasari Department of QC

elevating the lives of people and nature

Overview

Self Introduction

Work Plan (October 2018 – March 2019)

No.

Job Activities

Timeline

Remarks

1.

Physicochemical analysis

October 2018 – March 2019

QC analysis is follow production schedule

2.

Communicate with external labs and vendors

October 2018 – March 2019

Every time the sample is sent

3. 4.

Training - pesticide residue analysis January – March 2019 Document review October 2018 – March 2019

Job Activity Daily Activities

Additional Activities

 WTP Monitoring  WWTP Monitoring  WTP Chlorine Residue Monitoring

 Communicate with External Labs and Vendors  Pesticide Residue Analysis in External Lab

 Water and Nozzle Monitoring  Hand and Boots Sink Chlorine Residue Monitoring  Monitoring of Blancher Effectiveness

 Making, Reviewing, and Revising Documents (SOP, IK, and Form) for QC Department

Flowchart of Physicochemical Analysis

• Indirect Process Control

• Direct Process Control

Indirect Process Control

Manual Sampling



Transport samples to the lab

Sample Analysis

Monitoring of Blancher Effectiveness

Data Reporting

Data Interpretation

Direct Process Control

Manual Sampling

Sample Analysis



WTP Monitoring



WWTP Monitoring



WTP Chlorine Residue Monitoring



Water and Nozzle Monitoring



Hand and Foot Sink Chlorine Residue Monitoring

Data Interpretation

Data Reporting

Problem Analysis No

Problems

Causes

1.

Optical detection in paper based sensor for chlorine residue analysis is lack of accuracy and precision

- Unstable upon evaporation - Low resolution of color changing causes reading error

Effects Error in data reporting (false positive or false negative)

Solution Switch to another instrument or detection method

Remarks On progress

Future Planning No.

Job Activities

Timeline

Remarks

1.

Physicochemical analysis

April – September 2019

QC analysis is follow production schedule

2.

Communicate with external labs and vendors

April – September 2019

Every time the sample is sent

3.

Pesticide residue analysis in internal lab

Start at August 2019

4.

Document review

April – September 2019

Terima Kasih PT Austindo Nusantara Jaya Tbk Atrium Mulia, 3A Floor, Suite 3A-02 Jl. H.R. Rasuna Said Kav. B10-11 Jakarta 12910 - Indonesia T +62 21 29651777 F +62 21 29651788 www.anj-group.com

WTP Monitoring (RO Water)

WTP Monitoring (Treated Water)

WWTP Monitoring

Hand & Boots Sink Chlorine Residue Monitoring

Boots sterilize : 150200 ppm

Hand sterilize : 50100 ppm

Training – Pesticide Residue Analysis Analytical Method Validation & Quality Control in Pesticide Residue Analysis using Modified QuEChERS Method and LC/MS/MS

Sample Preparation (Homogenization)

Analyte Extraction (QuEChERS Method)

CCP : in a cryogenic or sub-ambient condition

CCP : -Addition of the extraction salt -Addition of the dSPE

Analyte Determination (Using LC/MS/MS) CCP : -Validation of Analytical Method

QuECheRS Method in Details