Gnn3 - D. Mancini, Usa

Department of Energy’s User Facilities for Nanoscience and Nanotechnology Derrick C. Mancini Project Manager and Nanofabrication Group Leader Center for Nanoscale Materials Argonne National Laboratory http://nano.anl.gov Global Nanotechnology Network May 26, 2005, Saarbrucken, Germany Pioneering Science and Technology

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

DOE BES Initiative for NanoScience & Technology: Nanoscale Science Research Centers DOE’s 5 NSRCs - http://www.sc.doe.gov/bes/NNI.htm •

Center for Nanophase Materials Sciences (ORNL)

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Molecular Foundry (LBNL)

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Center for Functional Nanomaterials (BNL)

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Center for Integrated Nanotechnologies (SNL-LANL)

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Center for Nanoscale Materials (ANL)

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Pioneering Science and Technology

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

DOE BES Initiative for NanoScience & Technology: Nanoscale Science Research Centers DOE’s 5 NSRCs • • • •

Each is a National User Facility Located at existing DOE National Laboratories Integrated with existing DOE National Facilities Provides a regional resource – – – – –

East Coast (Brookhaven National Lab) West Coast (Lawrence Berkeley National Lab) Southwest (Sandia & Los Alamos National Labs) South Central (Oak Ridge National Lab) North Central (Argonne National Lab)

• Scientific Research Mission - Themes • $18.5 M in DOE operating funds for each NSRC Pioneering Science and Technology

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

Center for Nanophase Materials Sciences

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A collaborative nanoscience user research facility at Oak Ridge National Laboratory in Tennessee for the synthesis, characterization, modeling, simulation, and design of nanoscale materials.

Integrated with: •Spallation Neutron Source •High Flux Isotope Reactor •Materials Analysis User Center

Building completed in spring 2005. http://www.cnms.ornl.gov/

Pioneering Science and Technology

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

Molecular Foundry World-class user facility at Lawrence Berkeley National Laboratory in California for the design, synthesis, and characterization of nanoscale materials. QuickTime™ and a TIFF (Uncompressed) decompressor are needed to see this picture.

Integrated with: •Advanced Light Source •National Center for Electron Microscopy •National Energy Research Scientific Computing Center

Building to be completed in spring 2006. http://foundry.lbl.gov/ Pioneering Science and Technology

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

Center for Integrated NanoTechnologies World-class research facilities at Sandia and Los Alamos National Laboratories in New Mexico for developing the scientific principles that govern the design, performance, and integration of nanoscale materials.

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Integrated with: •Integrated Materials Research Lab •Los Alamos Neutron Science Center •National High Magnetic Field Lab •Compound Semicon Research Lab •Microelectronics Development Lab QuickTime™ and a TIFF (Uncompressed) decompressor are needed to see this picture.

Building to be completed in fall 2005. http://cint.lanl.gov/

Pioneering Science and Technology

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

Center for Functional Nanomaterials World class facility at Brookhaven National Laboratory in New York for atomic level tailoring of a material's response to achieve a specific functionality. QuickTime™ and a TIFF (Uncompressed) decompressor are needed to see this picture.

Integrated with: •National Synchrotron Light Source •Laser Electron Accelerator Facility

• Building to be completed in spring 2007. http://www.cfn.bnl.gov/

Pioneering Science and Technology

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

Center for Nanoscale Materials World-class research facility at Argonne National Laboratory in Illinois for tackling the grand challenges of nanoscience.

• Unique $72M partnership • $36 M DOE funds • $36 M State-of-Illinois funds • Building to be completed in spring 2006 • $18.5 M DOE operations funds in FY 2007 http://nano.anl.gov/ Pioneering Science and Technology

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

Argonne’s Facilities for Nanoscience Center for Nanoscale Materials

‘One-stop’ User access to all ANL facilities

Electron Microscopy Center

The Electron Microscopy Center at Argonne National Laboratory Pioneering Science and Technology

Jazz – Teraflop Cluster th

DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

Center for Nanoscale Materials Mission • Enable world-class nanoscience aligned with the Department of Energy’s scientific vision. – Explore novel phenomena associated with the interplay between spatial, physical and chemical length scales and proximity effects. – Transform the art of nanomaterial and nanodevice fabrication into a science. – Understand the ultimate limits of miniaturization. – Lay foundations for new technologies based on the principles of nanoscience.

• Support users in doing outstanding science in a safe environment, by providing expertise and facilities to the nanoscience community. Pioneering Science and Technology

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

CNM’s User Program • Open access for all users. – Best science via peer-reviewed proposals (http://nano.anl.gov)

• Capabilities and facility shaped by CNM science. • Foster interactions across wide range of disciplines and professions. • Two phases – Early Access • Provide users access to existing ANL nanoscience capabilities. • 1st and 2nd Call for Proposals completed for time in 2004-2005 • 3rd Call for Proposals, July 15th deadline

– New Facilities • New building (funded by State of Illinois), to be constructed adjacent to the Advanced Photon Source. Construction start in June. • New equipment and Nanoprobe beamline (funded by DOE Nanoscale Science Research Centers program). Pioneering Science and Technology

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

Opportunities at the CNM • User program. – Individuals or group access to existing scientific capabilities/equipment in CNM. – Rapid access.

• ‘One-stop’ User access to all facilities at Argonne (APS, IPNS, EMC, advanced computing). • CNMs world-class staff. • Leverage large complement of advanced tools for nanoscience and nanotechnology. • Joint initiatives including workshops and funding. • Workforce training. • Working on new model for IP and tech transfer. – includes joint activities. – proprietary research at CNM (cost recovery fee). Pioneering Science and Technology

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

CNM Scientific Themes • Bio-inorganic interface (D. Tiede, T. Rajh, M. Firestone) • Nanocarbon (D. Gruen, J. Carlisle) • Nanomagnetism (S. Bader, A. Hoffmann) • Complex oxides (O. Auciello, S. Streiffer) • Nanophotonics (G. Wiederrecht, S. Gray) • Virtual Fab Lab (S. Gray, P. Zapol) Novel functional nanocomposites

Self-assembled functionalized arrays Pioneering Science and Technology

• Nanopatterning (D. Mancini, L. Ocola) • X-Ray Nanoprobe (J. Maser, B. Stephenson)

Sub-wavelength photon confinement/propagation th

DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

Nanomaterials for Energy at Argonne • Bio-inspired/biomimetic materials and processes Nanostructured 2D and 3D catalysis/photocatalysis; light harvesting, sensing and energy transduction; Protein-based materials for storage and transduction; Novel bio-inorganic composites; biomimetic; hydrogen production, storage and conversion.

biomimetic H-production

• Hydrogen Fuel Initiative (DOEs BES) • Nanoscale catalysis design Inorganic scaffolding for catalytic sites, eg., AAO membranes; Nanoscale phenomena – size, shape and curvature effects

Anodized Aluminum Oxide M. Pellin, et al.

• Nanostructured ‘materials by design’ for energy efficiency Ultra-strong magnets for efficient motors. Nanophotonics for > Tbps bandwidth. Nanocrystalline diamond for low-friction coatings.

• Theory and Modeling. Pioneering Science and Technology

Co/CoPt core-shell nanoparticle array

magnetization

inorganic membranes remanence (Mr)

saturation, (MS)

coercivity, (Hc)

magnetic field

Ultra-strong nanomagnet composites th

DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

Key Fabrication and Characterization Tools

LEO 1560XB CrossBeam

FIB/SEM

E-beam Lithography Pioneering Science and Technology

Plasma-enhanced CVD for Carbon

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

The Center for Nanoscale Materials Hard X-ray Nanoprobe at the APS

•Unique instrument to study individual nanostructures •30 nanometer spatial resolution or better •Quantitative structure, strain, magnetization •Sensitive trace element and chemical state analysis •Ability to penetrate overlayers, environments, fields Pioneering Science and Technology

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

Example of X-ray Fluorescence Imaging at the APS: TiO2-DNA Nanocomposites in Cells •

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Map Ti distribution using XRF, to quantify the success of transfection and visualize target of nanocomposite Affinity of transfected DNA for ribosomes causes localization to the nucleolus. CNM’s Hard X-ray Nanoprobe, at 30 nm resolution, will significantly improving applicability to cell biology.

TiO2-DNA Nanoparticles for in vivo Gene Surgery

G. Woloschak, Nature Materials 2, 343 (2003). (Northwestern/ANL collaboration)

DNA-nanoparticle crossing cell wall

Pioneering Science and Technology

X-ray elemental imaging of the cell chromosome showing location of the single stranded DNA-TiO2 nanoparticle

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

Advanced Photon Source

Pioneering Science and Technology

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

Advanced Photon Source

Pioneering Science and Technology

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

Center for Nanoscale Materials Building

•Adjacent to APS Sector 26 •Integrated with APS site design •Utilize APS site utilities Pioneering Science and Technology

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

Center for Nanoscale Materials Building ~85,000 gross square feet, including: •13,000 sq ft Laboratories •11,000 sq ft Cleanroom Facilities •33,000 sq ft Offices & Public Spaces

Pioneering Science and Technology

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

Center for Nanoscale Materials Building • CNM building complete in Spring ’06 • CNM Facility complete in Fall ’07 • 85,000 sq. ft. lab + office space

Pioneering Science and Technology

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

The Challenge: Enabling Access

• Coordinated Access • Distributed Access • Remote Access • Interactive Access • Telepresence • Telecollaboratory Pioneering Science and Technology

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

Telepresence & Telecollaboratory

• Platform Independent • Intuitive User Interface • Responsive to the User • Adaptable to Many Instruments • Provides user what they need to execute their experiments Pioneering Science and Technology

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

Telepresence & Telecollaboratory

Pioneering Science and Technology

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

Telepresence & Telecollaboratory

Neutron Residual Stress Facility at ORNL Pioneering Science and Technology

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

Telepresence & Telecollaboratory

TelePresence Microscopy Collaboratory, Advanced Microscopy Center at ANL Nestor Zalucek and Presistent Electronic Spaces Pioneering Science and Technology

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

Telepresence & Telecollaboratory

ANL

Univ. of Illinois ORNL

LBNL

Materials MicroCharacterization Laboratory Adoption of Web-based TPM Protocols Pioneering Science and Technology

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

Access Grid Nodes

Presenter mic

Presenter camera Ambient mic (tabletop)

Presenter mic

Presenter camera

Ambient mic (tabletop) Audience camera

Audience camera

Pioneering Science and Technology

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy

GNN and DOE User Facilities

• Information • Coordination • Education • Conferencing • Telepresence • Telecollaboratory Pioneering Science and Technology

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DOE NSRCs, GNN 2005, May 26

Office of Science U.S. Department of Energy