Air Sampling Techniques
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TYPES OF CHEMICAL 1 (Aqua Regia Ashing) 2 1,1,2-TRICHLORO-1,2,2-TRIFLUOROETHANE 3 1-NITROPYRENE IN DIESEL PARTICULATES 4 1-OCTANETHIOL 5 2,4-D 6 2-NITROPROPANE 7 ACETALDEHYDE by HPLC 8 ACETIC ACID 9 ACETIC ANHYDRIDE 10 ACETONITRILE 11 ACIDS, INORGANIC 12 ALCOHOLS COMBINED 13 ALCOHOLS II 14 ALCOHOLS III 15 ALCOHOLS IV 16 ALIPHATIC ALDEHYDES 17 ALKALINE DUSTS 18 AMINES, ALIPHATIC 19 AMINES, AROMATIC 20 AMINOETHANOL COMPOUNDS I 21 AMINOETHANOL COMPOUNDS II 22 AMMONIA 23 ANILINE, o-TOLUIDINE, AND NITROBENZENE 24 antimony* chromium* lithium potassium tin zirconium* 25 arsenic cobalt magnesium selenium titanium 26 ARSENIC TRIOXIDE 27 barium copper manganese silver tungsten* 28 beryllium iron* molybdenum strontium vanadium 29 BROMINE 30 cadmium lanthanum nickel tellurium yttrium 31 CHLORINATED AND ORGANONITROGEN HERBICIDES 32 CHLOROACETIC ACID 33 CHROMIUM, HEXAVALENT 34 CRESOL (all isomers) and PHENOL 35 DIAZOMETHANE 36 DICHLOROFLUOROMETHANE 37 DYES, BENZIDINE-, o-TOLIDINE-, o-DIANISIDINE 38 ELEMENTS by ICP 7301 39 ESTERS 1 40 ETHYL ACETATE 41 ETHYL BROMIDE 42 ETHYL CHLORIDE 43 ETHYL ETHER 44 ETHYLENE CHLOROHYDRIN 45 ETHYLENIMINE 46 FLUORIDES, aerosol and gas 47 FORMALDEHYDE 48 FORMALDEHYDE by GC
49 FORMIC ACID 50 GLUTARALDEHYDE 51 GLYCOL ETHERS 52 GLYCOLS 53 HEXACHLORO-1,3-CYCLOPENTADIENE 54 HEXACHLOROBUTADIENE 55 HYDRAZINE 56 HYDROCARBON HALOGENATED 57 HYDROCARBONS, AROMATIC 58 HYDROGEN CYANIDE 59 HYDROGEN SULFIDE 60 HYDROQUINONE 61 ISOCYANATES 62 ISOCYANATES, MONOMERIC 63 ISOPHORONE 64 ISOPROPYL ACETATE 65 ISOPROPYL ETHER 66 KEPONE 67 KETONES I 68 LEAD by Flame AAS 69 LEAD in Air by Chemical Spot Test 70 LEAD SULFIDE 71 MERCAPTANS, METHYL-, ETHYL-, and n-BUTYL 72 METHANOL 73 METHYL AND ETHYL METHACRYLATE 74 METHYL BROMIDE 75 METHYL CELLOSOLVE ACETATE 76 METHYL CHLORIDE 77 METHYL ETHYL KETON 78 METHYL ETHYL KETONE PEROXIDE 79 METHYL IODIDE 80 METHYL tert-BUTYL ETHER 81 METHYLENE CHLORIDE 82 METHYLTIN CHLORIDES 83 MONOMETHYLANILINE 84 MONOMETHYLHYDRAZINE 85 NAPHTHAS 86 NAPHTHAS 87 NAPHTHYLAMINES, a and b 88 NICKEL CARBONYL 89 NICOTINE 90 NITRIC OXIDE and NITROGEN DIOXIDE 91 NITROAROMATIC COMPOUNDS 92 NITROETHANE 93 NITROGLYCERIN 94 NITROMETHANE 95 NITROSAMINES 96 NITROUS OXIDE 97 OIL MIST, MINERAL 98 ORGANONITROGEN PESTICIDES
99 ORGANOPHOSPHORUS PESTICIDES 100 PHENYL ETHER 101 PHENYL GLYCIDYL ETHER 102 PHOSPHINE 103 p-NITROANILINE 104 POLYCYCLIC AROMATIC COMPOUNDS, TOTAL (PACs 105 POLYNUCLEAR AROMATIC HYDROCARBONS 106 POLYNUCLEAR AROMATIC HYDROCARBONS 107 PROPYLENE DICHLORIDE 108 PROPYLENE OXIDE 109 QUARTZ in coal mine dust, by IR (redeposition) 110 SILICA, CRYSTALLINE, 111 SULFUR DIOXIDE 112 SULFURYL FLUORIDE 113 SUPER ABSORBENT POLYMERS 114 TRIBUTYL PHOSPHATE 115 TRICHLOROETHYLENE 116 TRIFLUOROBROMOMETHANE 117 TUNGSTEN (soluble and insoluble) 118 VANADIUM OXIDES 119 VINYL ACETATE 120 VINYL BROMIDE 121 VINYL CHLORIDE 122 VINYLIDENE CHLORIDE 123 VOLATILE ORGANIC COMPOUNDS 124 WARFARIN 125 ZINC and compounds, as Zn 126 ZINC OXIDE
TYPES OF CHEMICAL 1 HYDROCARBON HALOGENATED 2 ALCOHOLS III 3 ALCOHOLS COMBINED 5 ACETIC ACID 6 CHLOROACETIC ACID
7 VOLATILE ORGANIC COMPOUNDS
8 KETONES I
9 ACETIC ANHYDRIDE
10 ACETALDEHYDE by HPLC
11 POLYNUCLEAR AROMATIC HYDROCARBONS
12 GLYCOLS
13 ORGANOPHOSPHORUS PESTICIDES
14 BROMINE
15 AMMONIA
16 1,1,2-TRICHLORO-1,2,2-TRIFLUOROETHANE
17 TRIFLUOROBROMOMETHANE
18 TUNGSTEN (soluble and insoluble)
19 TRICHLOROETHYLENE 20 TRIBUTYL PHOSPHATE
SILICA, CRYSTALLINE, 21
22 SULFUR DIOXIDE
23 SULFURYL FLUORIDE
24 POLYCYCLIC AROMATIC COMPOUNDS, TOTAL (PACs
25 SUPER ABSORBENT POLYMERS
26 GLYCOL ETHERS
27 PROPYLENE DICHLORIDE
28 QUARTZ in coal mine dust, by IR (redeposition)
29 ALIPHATIC ALDEHYDES
30 PHENYL GLYCIDYL ETHER
31 PHENYLHYDRAZINE
32 CRESOL (all isomers) and PHENOL
33 PHENYL ETHER
34 PHOSPHINE
35 ORGANONITROGEN PESTICIDES
36 OIL MIST, MINERAL
37 1-OCTANETHIOL
38 VOLATILE ORGANIC COMPOUNDS
39 p-NITROANILINE
40 NITROUS OXIDE
41 NITROSAMINES
42 1-NITROPYRENE IN DIESEL PARTICULATES
43 2-NITROPROPANE
44 NITROMETHANE
45 NITROGLYCERIN
46 NITROETHANE
47 ANILINE, o-TOLUIDINE, AND NITROBENZENE
48 NITROAROMATIC COMPOUNDS
49 NITRIC OXIDE and NITROGEN DIOXIDE
50 NICOTINE
51 NICKEL CARBONYL
52 NAPHTHYLAMINES, a and b
53 NAPHTHAS
54 METHYL tert-BUTYL ETHER
55 METHYL ETHYL KETONE PEROXIDE
56 MONOMETHYLHYDRAZINE
57 MONOMETHYLANILINE
58 METHYLTIN CHLORIDES
59 METHYL IODIDE
60 METHYL ETHYL KETON
61 METHYL CHLORIDE
62 METHYL BROMIDE
63 METHYL AND ETHYL METHACRYLATE
64 METHYL CELLOSOLVE ACETATE
65 METHANOL
66 LEAD SULFIDE
67 ELEMENTS by ICP 7301 (Aqua Regia Ashing) antimony* chromium* lithium potassium tin zirconium* arsenic cobalt magnesium selenium titanium barium copper manganese silver tungsten* beryllium iron* molybdenum strontium vanadium cadmium lanthanum nickel tellurium yttrium 68 ALKALINE DUSTS
69 LEAD in Air by Chemical Spot Test
70 LEAD by Flame AAS
71 KEPONE
72 NAPHTHAS
73 ISOPHORONE
74 ISOPROPYL ETHER
75 ISOPROPYL ACETATE
76 ISOCYANATES, MONOMERIC
77 ALCOHOLS II
78 HEXACHLOROBUTADIENE
79 HEXACHLORO-1,3-CYCLOPENTADIENE
80 HYDROQUINONE
81 HYDROGEN SULFIDE
82 HYDROGEN CYANIDE
83 HYDRAZINE
84 ISOCYANATES
85 ISOCYANATES
86 GLUTARALDEHYDE
87 FORMALDEHYDE by GC
88 POLYNUCLEAR AROMATIC HYDROCARBONS
89 FLUORIDES, aerosol and gas
90 FORMIC ACID
91 FORMALDEHYDE
92 PROPYLENE OXIDE
93 ETHYL BROMIDE
94 MERCAPTANS, METHYL-, ETHYL-, and n-BUTYL
95 ETHYL ETHER
96 ETHYLENIMINE
97 ESTERS 1
98 ETHYLENE CHLOROHYDRIN
99 HYDROCARBONS, AROMATIC
100 ETHYL CHLORIDE
ETHYL ACETATE 101
102 ALCOHOLS IV
AMINOETHANOL COMPOUNDS I 103
104 DYES, BENZIDINE-, o-TOLIDINE-, o-DIANISIDINE
105 DICHLOROFLUOROMETHANE
AMINES, ALIPHATIC 106
107 AMINOETHANOL COMPOUNDS II
METHYLENE CHLORIDE 108 109 DIAZOMETHANE
CHLORINATED AND ORGANONITROGEN HERBICIDES 110 111 2,4-D
112 CHROMIUM, HEXAVALENT
113 ACIDS, INORGANIC
114 ACETONITRILE
115 ARSENIC TRIOXIDE
VINYL CHLORIDE
VINYL BROMIDE
VINYLIDENE CHLORIDE
VINYL ACETATE
AMINES, AROMATIC
WARFARIN
ZINC and compounds, as Zn
ZINC OXIDE
VANADIUM OXIDES
SOBRENT TYPES SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg) SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg SOLID SORBENT TUBE (Coconut shell charcoal, 100 mg/50 mg) SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg) SOLID SORBENT TUBE (silica gel, 100 mg/50 mg) THERMAL DESORPTION TUBE (multi-bed sorbent tubes containing graphitized carbons and carbon molecular sieve sorbents [See Appendix]) SOLID SORBENT TUBE (Anasorb CMS, 150 mg/75 mg) LIQUID IN BUBBLER (mixed bubbler with 10 mL alkaline hydroxylamine) LIQUID IN BUBBLER (midget bubbler containing 15 mL Girard T solution @ pH 4.5) FILTER + SORBENT TUBE (37-mm, 2-μm, PTFE + washed XAD-2, 100 mg/50 mg) XAD-7 OVS tube (glass fiber filter, 13-mm; XAD-7, 200mg/100mg) FILTER/SOLID SORBENT TUBE (OVS-2 tube: 13-mm quartz filter; XAD-2, 270 mg/140 mg PREFILTER + FILTER (PTFE, 0.5-μm + silver membrane, 25-mm, 0.45-μm) SOLID SORBENT TUBE (sulfuric acid-treated silica gel) A 0.8-micron MCE prefilter may be used to remove particulate interferences.
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg SOLID SORBENT TUBES (two coconut shell charcoal tubes in series, 400 mg/200 mg and 100 mg/50 mg) FILTER (0.8-μm cellulose ester membrane SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg) FILTER (0.8-μm mixed cellulose ester membrane); above 23 C, use two filter cassettes in series CYCLONE + FILTER (10-mm cyclone, nylon or HigginsDewell (HD) + 0.8-:m MCE or 5-:m PVC) FILTER + TREATED FILTER (cellulose + Na2CO3; preceded by 0.8-μm cellulose ester membrane) SOLID SORBENT TUBE (coconut shell charcoal, 800 mg/200 mg) FILTER + SOLID SORBENT (2-μm, 37-mm, PTFE filter + washed XAD-2 resin, 100/50 mg ) MEMBRANE FILTER (PVC, 5-μm, 37-mm) SOLID SORBENT TUBE (Anasorb® 747, 140 mg/70 mg) SOLID SORBENT TUBE (petroleum charcoal, 100 mg/50 mg) CYCLONE + PREWEIGHED FILTER (10-mm cyclone, nylon or Higgins-Dewell (HD), and PVC filter, 37-mm, 5-μm) CARTRIDGE (containing silica gel coated with acidified 2,4-
dinitrophenylhydrazine)
SOLID SORBENT TUBE (coconut shell charcoal; 100 mg/50 mg) GLASS MIDGET BUBBLER (containing 15 mL 0.1 M hydrochloric acid) SOLID SORBENT TUBE (XAD-7, 100 mg/50 mg) CHARCOAL TUBE (coconut shell charcoal, 100 mg/50 mg) SORBENT TUBE (Hg(CN)2-coated silica gel, 300 mg/150 mg) FILTER/SOLID SORBENT TUBE (OVS-2 Tube: 13-mm quartz fiber filter; XAD-2, 270 mg/140 mg) MEMBRANE FILTER (37-mm diameter, 0.8-:m MCE, 5-:m PVC, 2-:m PTFE, or glass fiber) SOLID SORBENT TUBE (Tenax-GC, 100 mg/50 mg) THERMAL DESORPTION TUBE TECHNIQUE (multi-bed sorbent tubes containing graphitized carbons and carbon molecular sieve sorbents FILTER (0.8 μm mixed cellulose ester membrane AMBIENT AIR OR BAG SAMPLE
SOLID SORBENT TUBE (Thermosorb/N™ air sampler FILTER (Glass Fiber, 37-mm) SOLID SORBENT TUBE (Chromosorb 106, 100 mg/50 mg)
SOLID SORBENT TUBE (Chromosorb 106, 600 mg/300 mg) SOLID SAMPLER TUBE (Tenax-GC, 100 mg/50 mg) SOLID SORBENT TUBES (XAD-2, 600 mg + 300 mg) FILTER + SOLID SORBENT (Glass fiber filter, sulfuric acid treated + silica gel sorbent tube, 520/260 mg) SOLID SORBENT TUBE (Silica gel, 150 mg/75 mg) SORBENT TUBES (oxidizer + 2 triethanolamine-treated molecular sieve) SOLID SORBENT TUBE XAD-2 (100 mg/50 mg) PREFILTER + SOLID SORBENT TUBE (low-Ni charcoal, 120 mg/60 mg; 0.8-μm cellulose ester membrane FILTER + SOLID SORBENT (glass fiber + silica gel, 100 mg/50 mg) SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg) SOLID SORBENT TUBES (two charcoal tubes in series; front 400 mg; back 200 mg) IMPINGER (15 mL dimethyl phthalate) BUBBLER (0.1 M hydrochloric acid) MIDGET BUBBLER (0.05 M sulfuric acid, 10 mL) FILTER + SORBENT TUBE (OVS Tube: 13-mm glass fiber filter; XAD-2,
270/140 mg) SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg) SOLID SORBENT TUBE (beaded carbon, ~150 mg/~75 mg) SOLID SORBENT TUBES (two coconut shell charcoal tubes in series, 400 mg/200 mg and 100 mg/50 mg) SOLID SORBENT TUBES (two petroleum charcoal tubes, 400 mg and 200 mg; drying tube, 9-g Na2SO4, necessary at humidity >50%) SOLID SORBENT TUBE (XAD-2, 400/200 mg) SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg) SOLID SORBENT TUBE (silica gel, 100/50 mg) CYCLONE + FILTER (10-mm nylon or Higgins-Dewell (HD) cyclone
FILTER (0.8-μm, cellulose ester membrane, or 5.0-μm, polyvinyl chloride membrane
FILTER (1-μm PTFE membrane) FILTER (0.8-μm cellulose ester membrane) FILTER (0.8-μm cellulose ester membrane FILTER + IMPINGER (0.8-μm cellulose ester membrane + impinger with 0.1 M NaOH)
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg SOLID SORBENT TUBE (petroleum-based charcoal, 100 mg/50 mg) Solid Sorbent Tube (coconut shell charcoal; 100 mg/50 mg) SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg, IMPINGER (solution of 1-(2-methoxyphenyl)-piperazine in toluene) SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg) SOLID SORBENT TUBE (XAD-2; 100 mg/50 mg) SOLID SORBENT TUBE (2 tubes, Porapak T, 75 mg and 25 mg) FILTER (0.8-μm cellulose ester membrane FILTER + SOLID SORBENT TUBE (Zefluor, 0.5 μm; coconut shell charcoal, 400 mg/200 mg SOLID SORBENT TUBE (soda lime, 600 mg/200 mg) BUBBLER (15 mL 0.1 M HCl) IMPINGER (tryptamine/DMSO; 20 mL) IMPINGER (tryptamine/DMSO; 20 mL) SOLID SORBENT TUBE (silica gel coated with 2,4-dinitrophenylhydrazine HCl, 300 mg/150 mg
SOLID SORBENT TUBE (10% (2-hydroxymethyl)piperdine on XAD-2, 120 mg/60 mg FILTER + SORBENT (2-μm, 37-mm PTFE + washed XAD-2, 100 mg/50 mg) FILTER + TREATED PAD (0.8-μm cellulose ester membrane + Na2CO3-treated cellulose pad) FILTER + SOLID SORBENT TUBE (PTFE membrane, 5-μm + washed, silica gel, 400 mg/200 mg) CARTRIDGE (Cartridge containing silica gel coated with 2,4-dinitrophenylhydrazine) SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg) SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg) FILTER (glass fiber, 37-mm, impregnated with mercuric acetate) Solid Sorbent Tube (coconut shell charcoal, 100 mg/50 mg) BUBBLER (Folin's reagent SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg SOLID SORBENT TUBE (petroleum charcoal, 100 mg/50 mg) SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg) SOLID SORBENT TUBES (2 coconut shell charcoal tubes, 400 mg and 200 mg)
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg) SOLID SORBENT TUBE (Coconut shell charcoal, 100 mg/50 mg) SOLID SORBENT TUBE (silica gel, 300 mg/150 mg)
FILTER (5-μm PTFE membrane SOLID SORBENT TUBES (2 coconut shell charcoal tubes, 400 mg and 200 mg) SOLID SORBENT TUBE (silica gel, 150 mg / 75 mg)
IMPINGER (15 mL 2 mM hexanesulfonic acid) SOLID SORBENT (2 coconut shell charcoal tubes, 100/50 mg SOLID SORBENT TUBE (octanoic acid-coated XAD-2 resin, 100 mg/50 mg) FILTER/SOLID SORBENT TUBE (OVS tube: 11-mm quartz filter; XAD-2) FILTER (glass fiber, binderless FILTER (5.0-μm PVC membrane) SOLID SORBENT TUBE (washed silica gel, 400 mg/200 mg with glass fiber filter plug) SOLID SORBENT TUBE (coconut shell charcoal, 400/200 mg)
FILTER (Na2CO3-impregnated, 0.8-μm cellulose ester membrane + backup pad) SOLID SORBENT TUBE (2 tandem tubes, each with 150 mg activated coconut charcoal) SOLID SORBENT TUBE (coconut shell charcoal, 400 mg/200 mg) SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg) SOLID SORBENT TUBE (carbon molecular sieve; 160 mg/80 mg; ORBO-92 or equivalent) SOLID SORBENT TUBE (silica gel, 150 mg/75 mg) FILTER (1-μm PTFE membrane) FILTER (0.8-μm cellulose ester membrane FILTER (0.8-μm PVC membrane, 25-mm diameter, in open-face cassette) CYCLONE + FILTER (10-mm cyclone or Higgins-Dewell (HD) + 5-μm PVC membrane)
FLOW RATE
MEASUREMENT TECHNIQUE
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 1.0 L/min
GAS CHROMATOGRAPHY, FID
0.05 to 0.2 L/min
ION CHROMATOGRAPHY, CONDUCTIVITY DETECTION
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.2 to 1.0 L/min
VISIBLE ABSORPTION SPECTROPHOTOMETRY
0.1 to 0.5 L/min
HPLC, UV
2 L/min
HPLC, FLUORESCENCE/UV DETECTION
0.5 to 2 L/min
GAS CHROMATOGRAPHY, FID
0.2 to 1 L/min
GC, FLAME PHOTOMETRIC DETE
0.3 to 1 L/min
ION CHROMATOGRAPHY, CONDUCTIVITY
0.1 to 0.2 L/min
VISIBLE ABSORPTION SPECTROPHOTOMETRY
0.01 to 0.05 L/min
GAS CHROMATOGRAPH, FID
0.01 to 0.05 L/min
GAS CHROMATOGRAPHY, FID
1 to 4 L/min
ATOMIC ABSORPTION, FLAME
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
1 to 3 L/min
GC, FPD with a phosphorus filter
HD cyclone: 2.2 L/min; nylon cyclone: 1.7 L/min
VISIBLE ABSORPTION SPECTROPHOTOMETRY
0.5 to 1.5 L/min
ION CHROMATOGRAPHY
0.05 to 0.1 L/min
ION CHROMATOGRAPHY CONDUCTIVITY DETECTION
1 to 2 L/min
FLOW INJECTION, FLUORESCENCE DETECTOR
1 to 3 L/min
ICP-AES OR AAS
0.1 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
HD cyclone: 2.2 L/min nylon cyclone: 1.7 L/min
GAS CHROMATOGRAPHY WITH ELECTROLYTIC CONDUCTIVITY DETECTOR (HALL) INFRARED ABSORPTION SPECTROPHOTOMETRY (IR)
0.1 to 1.5 L/min
HPLC; UV DETECTION
0.01 to 0.2 L/min
0.01 to 1 L/min
GAS CHROMATOGRAPHY, FID
0.2 to 1 L/min
VISIBLE ABSORPTION SPECTROPHOTOMETRY
0.01 to 0.1 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.01 - 0.2 L/min
UV-VIS SPECTROMETER
0.1 to 1 L/min
HPLC, UV detection
1 to 3 L/min
INFRARED SPECTROPHOTOMETRY
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, SULFURSPECIFIC FPD
0.01 to 0.05 L/min
THERMAL DESORPTION, GAS CHROMATOGRAPHY, MASS SPECTROMETRY
1 to 3 L/min
HPLC, UV DETECTION
LONG-PATHLENGTH PORTABLE INFRARED SPECTROPHOTOMETER (FIELD READOUT 0.2 to 2 L/min
GAS CHROMATOGRAPHY,
1.0 to 2.0 L/min
GAS CHROMATOGRAPHY, NITROGEN CHEMILUMINESCENCE DETECTOR
0.01 to 0.05 L/min
GAS CHROMATOGRAPHY, FLAME IONIZATION DETECTOR
0.01 to 0.05 L/min
GAS CHROMATOGRAPHY, NITROGENSPECIFIC DETECTOR
0.2 to 1.0 L/min
GAS CHROMATOGRAPHY, ECD
0.01 to 0.05 L/min
GAS CHROMATOGRAPHY, FLAME IONIZATION DETECTOR
0.2 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.02 L/min
GAS CHROMATOGRAPHY, FID
NO: 0.025 L/min NO2: 0.025 - 0.2 L/min
VISIBLE ABSORPTION SPECTROPHOTOMETRY
1.0 L/min
GAS CHROMATOGRAPHY-NITROGEN PHOSPHOROUS DETECTOR
0.05 to 0.2 L/min
ATOMIC ABSORPTION, GRAPHITE FURNACE
0.2 to 0.8 L/min
GAS CHROMATOGRAPHY, FID ANALYTE
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.1 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.5 to 2 L/min
VISIBLE ABSORPTION SPECTROPHOTOMETRY
0.5 to 1.5 L/min
VISIBLE SPECTROPHOTOMETRY
0.2 to 1.0 L/min
GAS CHROMATOGRAPHY, FID
0.25 to 1 L/min
GAS CHROMATOGRAPHY, FPD
0.01 to 1 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FI
0.01 to 0.1 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.1 L/min
GAS CHROMATOGRAPHY, ATOMIC EMISSION DETECTION (GC-AED) monitoring Br, C and H channels
0.01 to 0.05 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FI
0.02 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
HD cyclone: 2.2 L/min nylon cyclone: 1.7 L/min
X-RAY POWDER DIFFRACTION
1 to 4 L/min
INDUCTIVELY COUPLED ARGON PLASMA, ATOMIC EMISSION SPECTROSCOPY (ICP-AES)
1 to 4 L/min
ACID-BASE TITRATION
2 L/min
CHEMICAL SPOT TEST KIT (Rhodizonate-based)
1 to 4 L/min
ATOMIC ABSORPTION SPECTROPHOTOMETER, FLAME
0.5 to 1 L/min
GAS CHROMATOGRAPHY, ECD
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 1 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.05 L/min
GAS CHROMATOGRAPHY, FID
0.02 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
1 L/min
HPLC, ELECTROCHEMICAL AND UV DETECTION
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.05 to 0.2 L/min
GAS CHROMATOGRAPHY/ECD
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, 63Ni ECD
1 to 4 L/min
HPLC, UV DETECTION
0.1 to 1.5 L/min ION CHROMATOGRAPHY, -RECOMMENDED: 0.2 L/minCONDUCTIVITY
0.05 to 0.2 L/min
SPECTROPHOTOMETRY, VISIBLE ABSORPTION
0.2 to 1.0 L/min
SPECTROPHOTOMETRY, VISIBLE ABSORPTION
1 to 2 L/min
HPLC, FLUORESCENCE DETECTOR/ ELECTROCHEMICAL DETECTOR
1 to 2 L/min
HPLC, FLUORESCENCE DETECTOR/ ELECTROCHEMICAL DETECTOR
0.05 to 0.5 L/min
HPLC, UV DETECTION
0.01 to 0.10 L/min
GAS CHROMATOGRAPHY, FID
2 L/min
GAS CHROMATOGRAPHY, CAPILLARY COLUMN, FID
1 to 2 L/min
ION-SPECIFIC ELECTRODE
0.05 to 0.2 L/min
ION CHROMATOGRAPHY, CONDUCTIVITY DETECTION
0.03 to 1.5 L/min
HPLC, UV DETECTION
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.1 to 0.2 L/min
GAS CHROMATOGRAPHY
0.01 to 0.2 L/min
GAS CHROMOTOGRAPHY, FID
0.2 L/min
HPLC, UV DETECTION
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
GAS CHROMATOGRAPHY, FID
0.02 to 0.05 L/min
SOLID SORBENT TUBES (2 coconut shell charcoal tubes,
400 mg and 200 mg) 0.01 to 0.2 L/minute
GAS CHROMATOGRAPHY, FID
0.01 to 0.05 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
1 to 3 L/min
HPLC, UV DETECTION
0.01 to 0.05 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 1.0 L/min
GAS CHROMATOGRAPHY, FID
0.5 to 1 L/min
ION CHROMATOGRAPHY, ion pairing
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.2 L/min
GAS CHROMATOGRAPHY, FID
0.2 to 1 L/min
GAS CHROMATOGRAPHY/ ELECTRON CAPTURE DETECTOR (GC/ECD)
1 to 3 L/min
HPLC, UV DETECTION
1 to 4 L/min
VISIBLE ABSORPTION SPECTROPHOTOMETRY
0.2 to 0.5 L/min
ION CHROMATOGRAPHY
GAS CHROMATOGRAPHY, FID 0.01 to 0.2 L/min
1 to 3 L/mi
ATOMIC ABSORPTION, GRAPHITE FURNACE
0.05 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.1 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
GAS CHROMATOGRAPHY, FID
1 to 4 L/min
HPLC, UV DETECTION
1 to 3 L/min
ATOMIC ABSORPTION, FLAME
1 to 3 L/min
X-RAY POWDER DIFFRACTION
HD cyclone: 2.2 L/min nylon cyclone: 1.7 L/min
X-RAY POWDER DIFFRACTION
TYPES OF CHEMICAL HYDROCARBON HALOGENATED
SOBRENT TYPES
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ALCOHOLS III
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ALCOHOLS COMBINED
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (Coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ACETIC ACID
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg)
0.01 to 1.0 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL CHLOROACETIC ACID
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (silica gel, 100 mg/50 mg)
0.05 to 0.2 L/min
MEASUREMENT TECHNIQUE ION CHROMATOGRAPHY, CONDUCTIVITY DETECTION
TYPES OF CHEMICAL KETONES I
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (Anasorb CMS, 150 mg/75 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ACETIC ANHYDRIDE
SAMPLING MEDIA
FLOW RATE
LIQUID IN BUBBLER (mixed bubbler with 10 mL alkaline hydroxylamine)
0.2 to 1.0 L/min
MEASUREMENT TECHNIQUE VISIBLE ABSORPTION SPECTROPHOTOMETRY
TYPES OF CHEMICAL ACETALDEHYDE by HPLC
SAMPLING MEDIA
FLOW RATE
LIQUID IN BUBBLER (midget bubbler containing 15 mL Girard T solution @ pH 4.5)
0.1 to 0.5 L/min
MEASUREMENT TECHNIQUE HPLC, UV
TYPES OF CHEMICAL POLYNUCLEAR AROMATIC HYDROCARBONS
SAMPLING MEDIA
FLOW RATE
FILTER + SORBENT TUBE (37-mm, 2-μm, PTFE + washed XAD-2, 100 mg/50 mg)
2 L/min
MEASUREMENT TECHNIQUE HPLC, FLUORESCENCE/UV DETECTION
TYPES OF CHEMICAL GLYCOLS
SAMPLING MEDIA
FLOW RATE
XAD-7 OVS tube (glass fiber filter, 13-mm; XAD-7, 200mg/100mg)
0.5 to 2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ORGANOPHOSPHORUS PESTICIDES
SAMPLING MEDIA
FLOW RATE
FILTER/SOLID SORBENT TUBE (OVS-2 tube: 13-mm quartz filter; XAD-2, 270 mg/140 mg
0.2 to 1 L/min
MEASUREMENT TECHNIQUE GC, FLAME PHOTOMETRIC DETE
TYPES OF CHEMICAL BROMINE
SAMPLING MEDIA
FLOW RATE
PREFILTER + FILTER (PTFE, 0.5-μm + silver membrane, 25-mm, 0.45-μm)
0.3 to 1 L/min
MEASUREMENT TECHNIQUE ION CHROMATOGRAPHY, CONDUCTIVITY
TYPES OF CHEMICAL AMMONIA
SAMPLING MEDIA SOLID SORBENT TUBE (sulfuric acid-treated silica gel) A 0.8-micron MCE prefilter may be used to remove particulate interferences.
FLOW RATE 0.1 to 0.2 L/min
MEASUREMENT TECHNIQUE VISIBLE ABSORPTION SPECTROPHOTOMETRY
TYPES OF CHEMICAL 1,1,2-TRICHLORO-1,2,2-TRIFLUOROETHANE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg
0.01 to 0.05 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPH, FID
TYPES OF CHEMICAL TRIFLUOROBROMOMETHANE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBES (two coconut shell charcoal tubes in series, 400 mg/200 mg and 100 mg/50 mg)
0.01 to 0.05 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL TUNGSTEN (soluble and insoluble)
SAMPLING MEDIA
FLOW RATE
FILTER (0.8-μm cellulose ester membrane
1 to 4 L/min
MEASUREMENT TECHNIQUE ATOMIC ABSORPTION, FLAME
TYPES OF CHEMICAL TRICHLOROETHYLENE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL TRIBUTYL PHOSPHATE
SAMPLING MEDIA
FLOW RATE
FILTER (0.8-μm mixed cellulose ester membrane); above 23 C, use two filter cassettes in series
1 to 3 L/min
MEASUREMENT TECHNIQUE GC, FPD with a phosphorus filter
TYPES OF CHEMICAL SILICA, CRYSTALLINE,
SAMPLING MEDIA
FLOW RATE
CYCLONE + FILTER (10-mm cyclone, nylon or HigginsDewell (HD) + 0.8-:m MCE or 5-:m PVC)
HD cyclone: 2.2 L/min; nylon cyclone: 1.7 L/min
MEASUREMENT TECHNIQUE VISIBLE ABSORPTION SPECTROPHOTOMETRY
TYPES OF CHEMICAL SULFUR DIOXIDE
SAMPLING MEDIA
FLOW RATE
FILTER + TREATED FILTER (cellulose + Na2CO3; preceded by 0.8-μm cellulose ester membrane)
0.5 to 1.5 L/min
MEASUREMENT TECHNIQUE ION CHROMATOGRAPHY
TYPES OF CHEMICAL SULFURYL FLUORIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 800 mg/200 mg)
0.05 to 0.1 L/min
MEASUREMENT TECHNIQUE ION CHROMATOGRAPHY CONDUCTIVITY DETECTION
TYPES OF CHEMICAL POLYCYCLIC AROMATIC COMPOUNDS, TOTAL (PACs
SAMPLING MEDIA
FLOW RATE
FILTER + SOLID SORBENT (2-μm, 37-mm, PTFE filter + washed XAD-2 resin, 100/50 mg )
1 to 2 L/min
MEASUREMENT TECHNIQUE FLOW INJECTION, FLUORESCENCE DETECTOR
TYPES OF CHEMICAL SUPER ABSORBENT POLYMERS
SAMPLING MEDIA
FLOW RATE
MEMBRANE FILTER (PVC, 5-μm, 37-mm)
1 to 3 L/min
MEASUREMENT TECHNIQUE ICP-AES OR AAS
TYPES OF CHEMICAL GLYCOL ETHERS
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (Anasorb® 747, 140 mg/70 mg)
0.1 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL PROPYLENE DICHLORIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (petroleum charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY WITH ELECTROLYTIC CONDUCTIVITY DETECTOR (HALL)
TYPES OF CHEMICAL QUARTZ in coal mine dust, by IR (redeposition)
SAMPLING MEDIA
FLOW RATE
CYCLONE + PREWEIGHED FILTER (10-mm cyclone, nylon or Higgins-Dewell (HD), and PVC filter, 37-mm, 5-μm)
HD cyclone: 2.2 L/min nylon cyclone: 1.7 L/min
MEASUREMENT TECHNIQUE INFRARED ABSORPTION SPECTROPHOTOMETRY (IR)
TYPES OF CHEMICAL ALIPHATIC ALDEHYDES
SAMPLING MEDIA
FLOW RATE
CARTRIDGE (containing silica gel coated with acidified 2,4dinitrophenylhydrazine)
0.1 to 1.5 L/min
MEASUREMENT TECHNIQUE HPLC; UV DETECTION
TYPES OF CHEMICAL PHENYL GLYCIDYL ETHER
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal; 100 mg/50 mg)
0.01 to 1 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL PHENYLHYDRAZINE
SAMPLING MEDIA
FLOW RATE
GLASS MIDGET BUBBLER (containing 15 mL 0.1 M hydrochloric acid)
0.2 to 1 L/min
MEASUREMENT TECHNIQUE VISIBLE ABSORPTION SPECTROPHOTOMETRY
TYPES OF CHEMICAL CRESOL (all isomers) and PHENOL
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (XAD-7, 100 mg/50 mg)
0.01 to 0.1 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL PHENYL ETHER
SAMPLING MEDIA
FLOW RATE
CHARCOAL TUBE (coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL PHOSPHINE
SAMPLING MEDIA
FLOW RATE
SORBENT TUBE (Hg(CN)2-coated silica gel, 300 mg/150 mg)
0.01 - 0.2 L/min
MEASUREMENT TECHNIQUE UV-VIS SPECTROMETER
TYPES OF CHEMICAL ORGANONITROGEN PESTICIDES
SAMPLING MEDIA
FLOW RATE
FILTER/SOLID SORBENT TUBE (OVS-2 Tube: 13-mm quartz fiber filter; XAD-2, 270 mg/140 mg)
0.1 to 1 L/min
MEASUREMENT TECHNIQUE HPLC, UV detection
TYPES OF CHEMICAL OIL MIST, MINERAL
SAMPLING MEDIA
FLOW RATE
MEMBRANE FILTER (37-mm diameter, 0.8-:m MCE, 5-:m PVC, 2-:m PTFE, or glass fiber)
1 to 3 L/min
MEASUREMENT TECHNIQUE INFRARED SPECTROPHOTOMETRY
TYPES OF CHEMICAL 1-OCTANETHIOL
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (Tenax-GC, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, SULFURSPECIFIC FPD
TYPES OF CHEMICAL VOLATILE ORGANIC COMPOUNDS
SAMPLING MEDIA
FLOW RATE
THERMAL DESORPTION TUBE TECHNIQUE (multi-bed sorbent tubes containing graphitized carbons and carbon molecular sieve sorbents
0.01 to 0.05 L/min
MEASUREMENT TECHNIQUE THERMAL DESORPTION, GAS CHROMATOGRAPHY, MASS SPECTROMETRY
TYPES OF CHEMICAL p-NITROANILINE
SAMPLING MEDIA
FLOW RATE
FILTER (0.8 μm mixed cellulose ester membrane
1 to 3 L/min
MEASUREMENT TECHNIQUE HPLC, UV DETECTION
TYPES OF CHEMICAL NITROUS OXIDE
SAMPLING MEDIA AMBIENT AIR OR BAG SAMPLE
FLOW RATE
MEASUREMENT TECHNIQUE LONG-PATHLENGTH PORTABLE INFRARED SPECTROPHOTOMETER (FIELD READOUT
TYPES OF CHEMICAL NITROSAMINES
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (Thermosorb/N™ air sampler
0.2 to 2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY,
TYPES OF CHEMICAL 1-NITROPYRENE IN DIESEL PARTICULATES
SAMPLING MEDIA
FLOW RATE
FILTER (Glass Fiber, 37-mm)
1.0 to 2.0 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, NITROGEN CHEMILUMINESCENCE DETECTOR
TYPES OF CHEMICAL 2-NITROPROPANE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (Chromosorb 106, 100 mg/50 mg)
0.01 to 0.05 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FLAME IONIZATION DETECTOR
TYPES OF CHEMICAL NITROMETHANE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (Chromosorb 106, 600 mg/300 mg)
0.01 to 0.05 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, NITROGENSPECIFIC DETECTOR
TYPES OF CHEMICAL NITROGLYCERIN
SAMPLING MEDIA
FLOW RATE
SOLID SAMPLER TUBE (Tenax-GC, 100 mg/50 mg)
0.2 to 1.0 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, ECD
TYPES OF CHEMICAL NITROETHANE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBES (XAD-2, 600 mg + 300 mg)
0.01 to 0.05 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FLAME IONIZATION DETECTOR
TYPES OF CHEMICAL ANILINE, o-TOLUIDINE, AND NITROBENZENE
SAMPLING MEDIA
FLOW RATE
FILTER + SOLID SORBENT (Glass fiber filter, sulfuric acid treated + silica gel sorbent tube, 520/260 mg)
0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL NITROAROMATIC COMPOUNDS
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (Silica gel, 150 mg/75 mg)
0.01 to 0.02 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL NITRIC OXIDE and NITROGEN DIOXIDE
SAMPLING MEDIA
FLOW RATE
SORBENT TUBES (oxidizer + 2 triethanolamine-treated molecular sieve)
NO: 0.025 L/min NO2: 0.025 - 0.2 L/min
MEASUREMENT TECHNIQUE VISIBLE ABSORPTION SPECTROPHOTOMETRY
TYPES OF CHEMICAL NICOTINE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE XAD-2 (100 mg/50 mg)
1.0 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY-NITROGEN PHOSPHOROUS DETECTOR
TYPES OF CHEMICAL NICKEL CARBONYL
SAMPLING MEDIA
FLOW RATE
PREFILTER + SOLID SORBENT TUBE (low-Ni charcoal, 120 mg/60 mg; 0.8-μm cellulose ester membrane
0.05 to 0.2 L/min
MEASUREMENT TECHNIQUE ATOMIC ABSORPTION, GRAPHITE FURNACE
TYPES OF CHEMICAL NAPHTHYLAMINES, a and b
SAMPLING MEDIA
FLOW RATE
FILTER + SOLID SORBENT (glass fiber + silica gel, 100 mg/50 mg)
0.2 to 0.8 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID ANALYTE
TYPES OF CHEMICAL NAPHTHAS
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL METHYL tert-BUTYL ETHER
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBES (two charcoal tubes in series; front 400 mg; back 200 mg)
0.1 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL METHYL ETHYL KETONE PEROXIDE
SAMPLING MEDIA
FLOW RATE
IMPINGER (15 mL dimethyl phthalate)
0.5 to 2 L/min
MEASUREMENT TECHNIQUE VISIBLE ABSORPTION SPECTROPHOTOMETRY
TYPES OF CHEMICAL MONOMETHYLHYDRAZINE
SAMPLING MEDIA
FLOW RATE
BUBBLER (0.1 M hydrochloric acid)
0.5 to 1.5 L/min
MEASUREMENT TECHNIQUE VISIBLE SPECTROPHOTOMETRY
TYPES OF CHEMICAL MONOMETHYLANILINE
SAMPLING MEDIA
FLOW RATE
MIDGET BUBBLER (0.05 M sulfuric acid, 10 mL)
0.2 to 1.0 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL METHYLTIN CHLORIDES
SAMPLING MEDIA
FLOW RATE
FILTER + SORBENT TUBE (OVS Tube: 13-mm glass fiber filter; XAD-2, 270/140 mg)
0.25 to 1 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FPD
TYPES OF CHEMICAL METHYL IODIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg)
0.01 to 1 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL METHYL ETHYL KETON
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (beaded carbon, ~150 mg/~75 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FI
TYPES OF CHEMICAL METHYL CHLORIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBES (two coconut shell charcoal tubes in series, 400 mg/200 mg and 100 mg/50 mg)
0.01 to 0.1 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL METHYL BROMIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBES (two petroleum charcoal tubes, 400 mg and 200 mg; drying tube, 9-g Na2SO4, necessary at humidity >50%)
0.01 to 0.1 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, ATOMIC EMISSION DETECTION (GC-AED) monitoring Br, C and H channels
TYPES OF CHEMICAL METHYL AND ETHYL METHACRYLATE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (XAD-2, 400/200 mg)
0.01 to 0.05 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL METHYL CELLOSOLVE ACETATE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FI
TYPES OF CHEMICAL METHANOL
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (silica gel, 100/50 mg)
0.02 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL LEAD SULFIDE
SAMPLING MEDIA
FLOW RATE
CYCLONE + FILTER (10-mm nylon or Higgins-Dewell (HD) cyclone
HD cyclone: 2.2 L/min nylon cyclone: 1.7 L/min
MEASUREMENT TECHNIQUE X-RAY POWDER DIFFRACTION
TYPES OF CHEMICAL ELEMENTS by ICP 7301 (Aqua Regia Ashing) antimony* chromium* lithium potassium tin zirconium* arsenic cobalt magnesium selenium titanium barium copper manganese silver tungsten* beryllium iron* molybdenum strontium vanadium cadmium lanthanum nickel tellurium yttrium
SAMPLING MEDIA
FLOW RATE
FILTER (0.8-μm, cellulose ester membrane, or 5.0-μm, polyvinyl chloride membrane
1 to 4 L/min
MEASUREMENT TECHNIQUE INDUCTIVELY COUPLED ARGON PLASMA, ATOMIC EMISSION SPECTROSCOPY (ICP-AES)
TYPES OF CHEMICAL ALKALINE DUSTS
SAMPLING MEDIA
FLOW RATE
FILTER (1-μm PTFE membrane)
1 to 4 L/min
MEASUREMENT TECHNIQUE ACID-BASE TITRATION
TYPES OF CHEMICAL LEAD in Air by Chemical Spot Test
SAMPLING MEDIA
FLOW RATE
FILTER (0.8-μm cellulose ester membrane)
2 L/min
MEASUREMENT TECHNIQUE CHEMICAL SPOT TEST KIT (Rhodizonate-based)
TYPES OF CHEMICAL LEAD by Flame AAS
SAMPLING MEDIA
FLOW RATE
FILTER (0.8-μm cellulose ester membrane
1 to 4 L/min
MEASUREMENT TECHNIQUE ATOMIC ABSORPTION SPECTROPHOTOMETER, FLAME
TYPES OF CHEMICAL KEPONE
SAMPLING MEDIA
FLOW RATE
FILTER + IMPINGER (0.8-μm cellulose ester membrane + impinger with 0.1 M NaOH)
0.5 to 1 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, ECD
TYPES OF CHEMICAL NAPHTHAS
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ISOPHORONE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (petroleum-based charcoal,
0.01 to 1 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ISOPROPYL ETHER
SAMPLING MEDIA
FLOW RATE
Solid Sorbent Tube (coconut shell charcoal; 100 mg/50 mg)
0.01 to 0.05 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ISOPROPYL ACETATE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg,
0.02 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ISOCYANATES, MONOMERIC
SAMPLING MEDIA
FLOW RATE
IMPINGER (solution of 1-(2-methoxyphenyl)-piperazine in toluene)
1 L/min
MEASUREMENT TECHNIQUE HPLC, ELECTROCHEMICAL AND UV DETECTION
TYPES OF CHEMICAL ALCOHOLS II
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL HEXACHLOROBUTADIENE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (XAD-2; 100 mg/50 mg)
0.05 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY/ECD
TYPES OF CHEMICAL HEXACHLORO-1,3-CYCLOPENTADIENE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (2 tubes, Porapak T, 75 mg and 25 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, 63Ni ECD
TYPES OF CHEMICAL HYDROQUINONE
SAMPLING MEDIA
FLOW RATE
FILTER (0.8-μm cellulose ester membrane
1 to 4 L/min
MEASUREMENT TECHNIQUE HPLC, UV DETECTION
TYPES OF CHEMICAL HYDROGEN SULFIDE
SAMPLING MEDIA
FLOW RATE
FILTER + SOLID SORBENT TUBE (Zefluor, 0.5 μm; coconut shell charcoal, 400 mg/200 mg
0.1 to 1.5 L/min -RECOMMENDED: 0.2 L/min
MEASUREMENT TECHNIQUE ION CHROMATOGRAPHY, CONDUCTIVITY
TYPES OF CHEMICAL HYDROGEN CYANIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (soda lime, 600 mg/200 mg)
0.05 to 0.2 L/min
MEASUREMENT TECHNIQUE SPECTROPHOTOMETRY, VISIBLE ABSORPTION
TYPES OF CHEMICAL HYDRAZINE
SAMPLING MEDIA
FLOW RATE
BUBBLER (15 mL 0.1 M HCl)
0.2 to 1.0 L/min
MEASUREMENT TECHNIQUE SPECTROPHOTOMETRY, VISIBLE ABSORPTION
TYPES OF CHEMICAL ISOCYANATES
SAMPLING MEDIA
FLOW RATE
IMPINGER (tryptamine/DMSO; 20 mL)
1 to 2 L/min
MEASUREMENT TECHNIQUE HPLC, FLUORESCENCE DETECTOR/ ELECTROCHEMICAL DETECTOR
TYPES OF CHEMICAL GLUTARALDEHYDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE 0.05 to 0.5 L/min (silica gel coated with 2,4-dinitrophenylhydrazine HCl, 300 mg/150 mg
MEASUREMENT TECHNIQUE HPLC, UV DETECTION
TYPES OF CHEMICAL FORMALDEHYDE by GC
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (10% (2-hydroxymethyl)piperdine on XAD-2, 120 mg/60 mg
0.01 to 0.10 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL POLYNUCLEAR AROMATIC HYDROCARBONS
SAMPLING MEDIA
FLOW RATE
FILTER + SORBENT (2-μm, 37-mm PTFE + washed XAD-2, 100 mg/50 mg)
2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, CAPILLARY COLUMN, FID
TYPES OF CHEMICAL FLUORIDES, aerosol and gas
SAMPLING MEDIA
FLOW RATE
FILTER + TREATED PAD (0.8-μm cellulose ester membrane + Na2CO3-treated cellulose pad)
1 to 2 L/min
MEASUREMENT TECHNIQUE ION-SPECIFIC ELECTRODE
TYPES OF CHEMICAL FORMIC ACID
SAMPLING MEDIA
FLOW RATE
FILTER + SOLID SORBENT TUBE (PTFE membrane, 5-μm + washed, silica gel, 400 mg/200 mg)
0.05 to 0.2 L/min
MEASUREMENT TECHNIQUE ION CHROMATOGRAPHY, CONDUCTIVITY DETECTION
TYPES OF CHEMICAL FORMALDEHYDE
SAMPLING MEDIA
FLOW RATE
CARTRIDGE (Cartridge containing silica gel coated with 2,4-dinitrophenylhydrazine)
0.03 to 1.5 L/min
MEASUREMENT TECHNIQUE HPLC, UV DETECTION
TYPES OF CHEMICAL PROPYLENE OXIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ETHYL BROMIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL MERCAPTANS, METHYL-, ETHYL-, and n-BUTYL
SAMPLING MEDIA
FLOW RATE
FILTER (glass fiber, 37-mm, impregnated with mercuric acetate)
0.1 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY
TYPES OF CHEMICAL ETHYL ETHER
SAMPLING MEDIA
FLOW RATE
Solid Sorbent Tube (coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMOTOGRAPHY, FID
TYPES OF CHEMICAL ETHYLENIMINE
SAMPLING MEDIA
FLOW RATE
BUBBLER (Folin's reagent
0.2 L/min
MEASUREMENT TECHNIQUE HPLC, UV DETECTION
TYPES OF CHEMICAL ESTERS 1
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ETHYLENE CHLOROHYDRIN
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (petroleum charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL HYDROCARBONS, AROMATIC
SAMPLING MEDIA SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg)
FLOW RATE
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ETHYL CHLORIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBES (2 coconut shell charcoal tubes, 400 mg and 200 mg)
0.02 to 0.05 L/min
MEASUREMENT TECHNIQUE SOLID SORBENT TUBES (2 coconut shell charcoal tubes, 400 mg and 200 mg)
TYPES OF CHEMICAL ETHYL ACETATE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.2 L/minute
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ALCOHOLS IV
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (Coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.05 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL AMINOETHANOL COMPOUNDS I
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (silica gel, 300 mg/150 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL DYES, BENZIDINE-, o-TOLIDINE-, o-DIANISIDINE
SAMPLING MEDIA
FLOW RATE
FILTER (5-μm PTFE membrane
1 to 3 L/min
MEASUREMENT TECHNIQUE HPLC, UV DETECTION
TYPES OF CHEMICAL DICHLOROFLUOROMETHANE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBES (2 coconut shell charcoal tubes, 400 mg and 200 mg)
0.01 to 0.05 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL AMINES, ALIPHATIC
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (silica gel, 150 mg / 75 mg)
0.01 to 1.0 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL AMINOETHANOL COMPOUNDS II
SAMPLING MEDIA
FLOW RATE
IMPINGER (15 mL 2 mM hexanesulfonic acid)
0.5 to 1 L/min
MEASUREMENT TECHNIQUE ION CHROMATOGRAPHY, ion pairing
TYPES OF CHEMICAL METHYLENE CHLORIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT (2 coconut shell charcoal tubes, 100/50 mg
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL DIAZOMETHANE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (octanoic acid-coated XAD-2 resin, 100 mg/50 mg)
0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL CHLORINATED AND ORGANONITROGEN HERBICIDES
SAMPLING MEDIA
FLOW RATE
FILTER/SOLID SORBENT TUBE (OVS tube: 11-mm quartz filter; XAD-2)
0.2 to 1 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY/ ELECTRON CAPTURE DETECTOR (GC/ECD)
TYPES OF CHEMICAL 2,4-D
SAMPLING MEDIA
FLOW RATE
FILTER (glass fiber, binderless
1 to 3 L/min
MEASUREMENT TECHNIQUE HPLC, UV DETECTION
TYPES OF CHEMICAL CHROMIUM, HEXAVALENT
SAMPLING MEDIA
FLOW RATE
FILTER (5.0-μm PVC membrane)
1 to 4 L/min
MEASUREMENT TECHNIQUE VISIBLE ABSORPTION SPECTROPHOTOMETRY
TYPES OF CHEMICAL ACIDS, INORGANIC
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (washed silica gel, 400 mg/200 mg with glass fiber filter plug)
0.2 to 0.5 L/min
MEASUREMENT TECHNIQUE ION CHROMATOGRAPHY
TYPES OF CHEMICAL ACETONITRILE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 400/200 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ARSENIC TRIOXIDE
SAMPLING MEDIA FILTER (Na2CO3-impregnated, 0.8-μm cellulose ester membrane + backup pad)
FLOW RATE
MEASUREMENT TECHNIQUE
1 to 3 L/mi
ATOMIC ABSORPTION, GRAPHITE FURNACE
TYPES OF CHEMICAL VANADIUM OXIDES
SAMPLING MEDIA
FLOW RATE
CYCLONE + FILTER (10-mm cyclone or Higgins-Dewell (HD) + 5-μm PVC membrane)
HD cyclone: 2.2 L/min nylon cyclone: 1.7 L/min
MEASUREMENT TECHNIQUE X-RAY POWDER DIFFRACTION
TYPES OF CHEMICAL ZINC OXIDE
SAMPLING MEDIA
FLOW RATE
FILTER (0.8-μm PVC membrane, 25-mm diameter, in open-face cassette)
1 to 3 L/min
MEASUREMENT TECHNIQUE X-RAY POWDER DIFFRACTION
TYPES OF CHEMICAL ZINC and compounds, as Zn
SAMPLING MEDIA
FLOW RATE
FILTER (0.8-μm cellulose ester membrane
1 to 3 L/min
MEASUREMENT TECHNIQUE ATOMIC ABSORPTION, FLAME
TYPES OF CHEMICAL WARFARIN
SAMPLING MEDIA
FLOW RATE
FILTER (1-μm PTFE membrane)
1 to 4 L/min
MEASUREMENT TECHNIQUE HPLC, UV DETECTION
TYPES OF CHEMICAL AMINES, AROMATIC
SAMPLING MEDIA SOLID SORBENT TUBE (silica gel, 150 mg/75 mg)
FLOW RATE
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL VINYL ACETATE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (carbon molecular sieve; 160 mg/80 mg; ORBO-92 or equivalent)
0.1 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL VINYLIDENE CHLORIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL VINYL BROMIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 400 mg/200 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL VINYL CHLORIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (2 tandem tubes, each with 150 mg activated coconut charcoal)
0.05 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL 1 (Aqua Regia Ashing) 2 1,1,2-TRICHLORO-1,2,2-TRIFLUOROETHANE 3 1-NITROPYRENE IN DIESEL PARTICULATES 4 1-OCTANETHIOL 5 2,4-D 6 2-NITROPROPANE 7 ACETALDEHYDE by HPLC 8 ACETIC ACID 9 ACETIC ANHYDRIDE 10 ACETONITRILE 11 ACIDS, INORGANIC 12 ALCOHOLS COMBINED 13 ALCOHOLS II 14 ALCOHOLS III 15 ALCOHOLS IV 16 ALIPHATIC ALDEHYDES 17 ALKALINE DUSTS 18 AMINES, ALIPHATIC 19 AMINES, AROMATIC 20 AMINOETHANOL COMPOUNDS I 21 AMINOETHANOL COMPOUNDS II 22 AMMONIA 23 ANILINE, o-TOLUIDINE, AND NITROBENZENE 24 antimony* chromium* lithium potassium tin zirconium* 25 arsenic cobalt magnesium selenium titanium 26 ARSENIC TRIOXIDE 27 barium copper manganese silver tungsten* 28 beryllium iron* molybdenum strontium vanadium 29 BROMINE 30 cadmium lanthanum nickel tellurium yttrium 31 CHLORINATED AND ORGANONITROGEN HERBICIDES 32 CHLOROACETIC ACID 33 CHROMIUM, HEXAVALENT 34 CRESOL (all isomers) and PHENOL 35 DIAZOMETHANE 36 DICHLOROFLUOROMETHANE 37 DYES, BENZIDINE-, o-TOLIDINE-, o-DIANISIDINE 38 ELEMENTS by ICP 7301 39 ESTERS 1 40 ETHYL ACETATE 41 ETHYL BROMIDE 42 ETHYL CHLORIDE 43 ETHYL ETHER 44 ETHYLENE CHLOROHYDRIN 45 ETHYLENIMINE 46 FLUORIDES, aerosol and gas 47 FORMALDEHYDE 48 FORMALDEHYDE by GC
49 FORMIC ACID 50 GLUTARALDEHYDE 51 GLYCOL ETHERS 52 GLYCOLS 53 HEXACHLORO-1,3-CYCLOPENTADIENE 54 HEXACHLOROBUTADIENE 55 HYDRAZINE 56 HYDROCARBON HALOGENATED 57 HYDROCARBONS, AROMATIC 58 HYDROGEN CYANIDE 59 HYDROGEN SULFIDE 60 HYDROQUINONE 61 ISOCYANATES 62 ISOCYANATES, MONOMERIC 63 ISOPHORONE 64 ISOPROPYL ACETATE 65 ISOPROPYL ETHER 66 KEPONE 67 KETONES I 68 LEAD by Flame AAS 69 LEAD in Air by Chemical Spot Test 70 LEAD SULFIDE 71 MERCAPTANS, METHYL-, ETHYL-, and n-BUTYL 72 METHANOL 73 METHYL AND ETHYL METHACRYLATE 74 METHYL BROMIDE 75 METHYL CELLOSOLVE ACETATE 76 METHYL CHLORIDE 77 METHYL ETHYL KETON 78 METHYL ETHYL KETONE PEROXIDE 79 METHYL IODIDE 80 METHYL tert-BUTYL ETHER 81 METHYLENE CHLORIDE 82 METHYLTIN CHLORIDES 83 MONOMETHYLANILINE 84 MONOMETHYLHYDRAZINE 85 NAPHTHAS 86 NAPHTHAS 87 NAPHTHYLAMINES, a and b 88 NICKEL CARBONYL 89 NICOTINE 90 NITRIC OXIDE and NITROGEN DIOXIDE 91 NITROAROMATIC COMPOUNDS 92 NITROETHANE 93 NITROGLYCERIN 94 NITROMETHANE 95 NITROSAMINES 96 NITROUS OXIDE 97 OIL MIST, MINERAL 98 ORGANONITROGEN PESTICIDES
99 ORGANOPHOSPHORUS PESTICIDES 100 PHENYL ETHER 101 PHENYL GLYCIDYL ETHER 102 PHOSPHINE 103 p-NITROANILINE 104 POLYCYCLIC AROMATIC COMPOUNDS, TOTAL (PACs 105 POLYNUCLEAR AROMATIC HYDROCARBONS 106 POLYNUCLEAR AROMATIC HYDROCARBONS 107 PROPYLENE DICHLORIDE 108 PROPYLENE OXIDE 109 QUARTZ in coal mine dust, by IR (redeposition) 110 SILICA, CRYSTALLINE, 111 SULFUR DIOXIDE 112 SULFURYL FLUORIDE 113 SUPER ABSORBENT POLYMERS 114 TRIBUTYL PHOSPHATE 115 TRICHLOROETHYLENE 116 TRIFLUOROBROMOMETHANE 117 TUNGSTEN (soluble and insoluble) 118 VANADIUM OXIDES 119 VINYL ACETATE 120 VINYL BROMIDE 121 VINYL CHLORIDE 122 VINYLIDENE CHLORIDE 123 VOLATILE ORGANIC COMPOUNDS 124 WARFARIN 125 ZINC and compounds, as Zn 126 ZINC OXIDE
TYPES OF CHEMICAL 1 HYDROCARBON HALOGENATED 2 ALCOHOLS III 3 ALCOHOLS COMBINED 5 ACETIC ACID 6 CHLOROACETIC ACID
7 VOLATILE ORGANIC COMPOUNDS
8 KETONES I
9 ACETIC ANHYDRIDE
10 ACETALDEHYDE by HPLC
11 POLYNUCLEAR AROMATIC HYDROCARBONS
12 GLYCOLS
13 ORGANOPHOSPHORUS PESTICIDES
14 BROMINE
15 AMMONIA
16 1,1,2-TRICHLORO-1,2,2-TRIFLUOROETHANE
17 TRIFLUOROBROMOMETHANE
18 TUNGSTEN (soluble and insoluble)
19 TRICHLOROETHYLENE 20 TRIBUTYL PHOSPHATE
SILICA, CRYSTALLINE, 21
22 SULFUR DIOXIDE
23 SULFURYL FLUORIDE
24 POLYCYCLIC AROMATIC COMPOUNDS, TOTAL (PACs
25 SUPER ABSORBENT POLYMERS
26 GLYCOL ETHERS
27 PROPYLENE DICHLORIDE
28 QUARTZ in coal mine dust, by IR (redeposition)
29 ALIPHATIC ALDEHYDES
30 PHENYL GLYCIDYL ETHER
31 PHENYLHYDRAZINE
32 CRESOL (all isomers) and PHENOL
33 PHENYL ETHER
34 PHOSPHINE
35 ORGANONITROGEN PESTICIDES
36 OIL MIST, MINERAL
37 1-OCTANETHIOL
38 VOLATILE ORGANIC COMPOUNDS
39 p-NITROANILINE
40 NITROUS OXIDE
41 NITROSAMINES
42 1-NITROPYRENE IN DIESEL PARTICULATES
43 2-NITROPROPANE
44 NITROMETHANE
45 NITROGLYCERIN
46 NITROETHANE
47 ANILINE, o-TOLUIDINE, AND NITROBENZENE
48 NITROAROMATIC COMPOUNDS
49 NITRIC OXIDE and NITROGEN DIOXIDE
50 NICOTINE
51 NICKEL CARBONYL
52 NAPHTHYLAMINES, a and b
53 NAPHTHAS
54 METHYL tert-BUTYL ETHER
55 METHYL ETHYL KETONE PEROXIDE
56 MONOMETHYLHYDRAZINE
57 MONOMETHYLANILINE
58 METHYLTIN CHLORIDES
59 METHYL IODIDE
60 METHYL ETHYL KETON
61 METHYL CHLORIDE
62 METHYL BROMIDE
63 METHYL AND ETHYL METHACRYLATE
64 METHYL CELLOSOLVE ACETATE
65 METHANOL
66 LEAD SULFIDE
67 ELEMENTS by ICP 7301 (Aqua Regia Ashing) antimony* chromium* lithium potassium tin zirconium* arsenic cobalt magnesium selenium titanium barium copper manganese silver tungsten* beryllium iron* molybdenum strontium vanadium cadmium lanthanum nickel tellurium yttrium 68 ALKALINE DUSTS
69 LEAD in Air by Chemical Spot Test
70 LEAD by Flame AAS
71 KEPONE
72 NAPHTHAS
73 ISOPHORONE
74 ISOPROPYL ETHER
75 ISOPROPYL ACETATE
76 ISOCYANATES, MONOMERIC
77 ALCOHOLS II
78 HEXACHLOROBUTADIENE
79 HEXACHLORO-1,3-CYCLOPENTADIENE
80 HYDROQUINONE
81 HYDROGEN SULFIDE
82 HYDROGEN CYANIDE
83 HYDRAZINE
84 ISOCYANATES
85 ISOCYANATES
86 GLUTARALDEHYDE
87 FORMALDEHYDE by GC
88 POLYNUCLEAR AROMATIC HYDROCARBONS
89 FLUORIDES, aerosol and gas
90 FORMIC ACID
91 FORMALDEHYDE
92 PROPYLENE OXIDE
93 ETHYL BROMIDE
94 MERCAPTANS, METHYL-, ETHYL-, and n-BUTYL
95 ETHYL ETHER
96 ETHYLENIMINE
97 ESTERS 1
98 ETHYLENE CHLOROHYDRIN
99 HYDROCARBONS, AROMATIC
100 ETHYL CHLORIDE
ETHYL ACETATE 101
102 ALCOHOLS IV
AMINOETHANOL COMPOUNDS I 103
104 DYES, BENZIDINE-, o-TOLIDINE-, o-DIANISIDINE
105 DICHLOROFLUOROMETHANE
AMINES, ALIPHATIC 106
107 AMINOETHANOL COMPOUNDS II
METHYLENE CHLORIDE 108 109 DIAZOMETHANE
CHLORINATED AND ORGANONITROGEN HERBICIDES 110 111 2,4-D
112 CHROMIUM, HEXAVALENT
113 ACIDS, INORGANIC
114 ACETONITRILE
115 ARSENIC TRIOXIDE
VINYL CHLORIDE
VINYL BROMIDE
VINYLIDENE CHLORIDE
VINYL ACETATE
AMINES, AROMATIC
WARFARIN
ZINC and compounds, as Zn
ZINC OXIDE
VANADIUM OXIDES
SOBRENT TYPES SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg) SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg SOLID SORBENT TUBE (Coconut shell charcoal, 100 mg/50 mg) SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg) SOLID SORBENT TUBE (silica gel, 100 mg/50 mg) THERMAL DESORPTION TUBE (multi-bed sorbent tubes containing graphitized carbons and carbon molecular sieve sorbents [See Appendix]) SOLID SORBENT TUBE (Anasorb CMS, 150 mg/75 mg) LIQUID IN BUBBLER (mixed bubbler with 10 mL alkaline hydroxylamine) LIQUID IN BUBBLER (midget bubbler containing 15 mL Girard T solution @ pH 4.5) FILTER + SORBENT TUBE (37-mm, 2-μm, PTFE + washed XAD-2, 100 mg/50 mg) XAD-7 OVS tube (glass fiber filter, 13-mm; XAD-7, 200mg/100mg) FILTER/SOLID SORBENT TUBE (OVS-2 tube: 13-mm quartz filter; XAD-2, 270 mg/140 mg PREFILTER + FILTER (PTFE, 0.5-μm + silver membrane, 25-mm, 0.45-μm) SOLID SORBENT TUBE (sulfuric acid-treated silica gel) A 0.8-micron MCE prefilter may be used to remove particulate interferences.
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg SOLID SORBENT TUBES (two coconut shell charcoal tubes in series, 400 mg/200 mg and 100 mg/50 mg) FILTER (0.8-μm cellulose ester membrane SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg) FILTER (0.8-μm mixed cellulose ester membrane); above 23 C, use two filter cassettes in series CYCLONE + FILTER (10-mm cyclone, nylon or HigginsDewell (HD) + 0.8-:m MCE or 5-:m PVC) FILTER + TREATED FILTER (cellulose + Na2CO3; preceded by 0.8-μm cellulose ester membrane) SOLID SORBENT TUBE (coconut shell charcoal, 800 mg/200 mg) FILTER + SOLID SORBENT (2-μm, 37-mm, PTFE filter + washed XAD-2 resin, 100/50 mg ) MEMBRANE FILTER (PVC, 5-μm, 37-mm) SOLID SORBENT TUBE (Anasorb® 747, 140 mg/70 mg) SOLID SORBENT TUBE (petroleum charcoal, 100 mg/50 mg) CYCLONE + PREWEIGHED FILTER (10-mm cyclone, nylon or Higgins-Dewell (HD), and PVC filter, 37-mm, 5-μm) CARTRIDGE (containing silica gel coated with acidified 2,4-
dinitrophenylhydrazine)
SOLID SORBENT TUBE (coconut shell charcoal; 100 mg/50 mg) GLASS MIDGET BUBBLER (containing 15 mL 0.1 M hydrochloric acid) SOLID SORBENT TUBE (XAD-7, 100 mg/50 mg) CHARCOAL TUBE (coconut shell charcoal, 100 mg/50 mg) SORBENT TUBE (Hg(CN)2-coated silica gel, 300 mg/150 mg) FILTER/SOLID SORBENT TUBE (OVS-2 Tube: 13-mm quartz fiber filter; XAD-2, 270 mg/140 mg) MEMBRANE FILTER (37-mm diameter, 0.8-:m MCE, 5-:m PVC, 2-:m PTFE, or glass fiber) SOLID SORBENT TUBE (Tenax-GC, 100 mg/50 mg) THERMAL DESORPTION TUBE TECHNIQUE (multi-bed sorbent tubes containing graphitized carbons and carbon molecular sieve sorbents FILTER (0.8 μm mixed cellulose ester membrane AMBIENT AIR OR BAG SAMPLE
SOLID SORBENT TUBE (Thermosorb/N™ air sampler FILTER (Glass Fiber, 37-mm) SOLID SORBENT TUBE (Chromosorb 106, 100 mg/50 mg)
SOLID SORBENT TUBE (Chromosorb 106, 600 mg/300 mg) SOLID SAMPLER TUBE (Tenax-GC, 100 mg/50 mg) SOLID SORBENT TUBES (XAD-2, 600 mg + 300 mg) FILTER + SOLID SORBENT (Glass fiber filter, sulfuric acid treated + silica gel sorbent tube, 520/260 mg) SOLID SORBENT TUBE (Silica gel, 150 mg/75 mg) SORBENT TUBES (oxidizer + 2 triethanolamine-treated molecular sieve) SOLID SORBENT TUBE XAD-2 (100 mg/50 mg) PREFILTER + SOLID SORBENT TUBE (low-Ni charcoal, 120 mg/60 mg; 0.8-μm cellulose ester membrane FILTER + SOLID SORBENT (glass fiber + silica gel, 100 mg/50 mg) SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg) SOLID SORBENT TUBES (two charcoal tubes in series; front 400 mg; back 200 mg) IMPINGER (15 mL dimethyl phthalate) BUBBLER (0.1 M hydrochloric acid) MIDGET BUBBLER (0.05 M sulfuric acid, 10 mL) FILTER + SORBENT TUBE (OVS Tube: 13-mm glass fiber filter; XAD-2,
270/140 mg) SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg) SOLID SORBENT TUBE (beaded carbon, ~150 mg/~75 mg) SOLID SORBENT TUBES (two coconut shell charcoal tubes in series, 400 mg/200 mg and 100 mg/50 mg) SOLID SORBENT TUBES (two petroleum charcoal tubes, 400 mg and 200 mg; drying tube, 9-g Na2SO4, necessary at humidity >50%) SOLID SORBENT TUBE (XAD-2, 400/200 mg) SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg) SOLID SORBENT TUBE (silica gel, 100/50 mg) CYCLONE + FILTER (10-mm nylon or Higgins-Dewell (HD) cyclone
FILTER (0.8-μm, cellulose ester membrane, or 5.0-μm, polyvinyl chloride membrane
FILTER (1-μm PTFE membrane) FILTER (0.8-μm cellulose ester membrane) FILTER (0.8-μm cellulose ester membrane FILTER + IMPINGER (0.8-μm cellulose ester membrane + impinger with 0.1 M NaOH)
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg SOLID SORBENT TUBE (petroleum-based charcoal, 100 mg/50 mg) Solid Sorbent Tube (coconut shell charcoal; 100 mg/50 mg) SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg, IMPINGER (solution of 1-(2-methoxyphenyl)-piperazine in toluene) SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg) SOLID SORBENT TUBE (XAD-2; 100 mg/50 mg) SOLID SORBENT TUBE (2 tubes, Porapak T, 75 mg and 25 mg) FILTER (0.8-μm cellulose ester membrane FILTER + SOLID SORBENT TUBE (Zefluor, 0.5 μm; coconut shell charcoal, 400 mg/200 mg SOLID SORBENT TUBE (soda lime, 600 mg/200 mg) BUBBLER (15 mL 0.1 M HCl) IMPINGER (tryptamine/DMSO; 20 mL) IMPINGER (tryptamine/DMSO; 20 mL) SOLID SORBENT TUBE (silica gel coated with 2,4-dinitrophenylhydrazine HCl, 300 mg/150 mg
SOLID SORBENT TUBE (10% (2-hydroxymethyl)piperdine on XAD-2, 120 mg/60 mg FILTER + SORBENT (2-μm, 37-mm PTFE + washed XAD-2, 100 mg/50 mg) FILTER + TREATED PAD (0.8-μm cellulose ester membrane + Na2CO3-treated cellulose pad) FILTER + SOLID SORBENT TUBE (PTFE membrane, 5-μm + washed, silica gel, 400 mg/200 mg) CARTRIDGE (Cartridge containing silica gel coated with 2,4-dinitrophenylhydrazine) SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg) SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg) FILTER (glass fiber, 37-mm, impregnated with mercuric acetate) Solid Sorbent Tube (coconut shell charcoal, 100 mg/50 mg) BUBBLER (Folin's reagent SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg SOLID SORBENT TUBE (petroleum charcoal, 100 mg/50 mg) SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg) SOLID SORBENT TUBES (2 coconut shell charcoal tubes, 400 mg and 200 mg)
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg) SOLID SORBENT TUBE (Coconut shell charcoal, 100 mg/50 mg) SOLID SORBENT TUBE (silica gel, 300 mg/150 mg)
FILTER (5-μm PTFE membrane SOLID SORBENT TUBES (2 coconut shell charcoal tubes, 400 mg and 200 mg) SOLID SORBENT TUBE (silica gel, 150 mg / 75 mg)
IMPINGER (15 mL 2 mM hexanesulfonic acid) SOLID SORBENT (2 coconut shell charcoal tubes, 100/50 mg SOLID SORBENT TUBE (octanoic acid-coated XAD-2 resin, 100 mg/50 mg) FILTER/SOLID SORBENT TUBE (OVS tube: 11-mm quartz filter; XAD-2) FILTER (glass fiber, binderless FILTER (5.0-μm PVC membrane) SOLID SORBENT TUBE (washed silica gel, 400 mg/200 mg with glass fiber filter plug) SOLID SORBENT TUBE (coconut shell charcoal, 400/200 mg)
FILTER (Na2CO3-impregnated, 0.8-μm cellulose ester membrane + backup pad) SOLID SORBENT TUBE (2 tandem tubes, each with 150 mg activated coconut charcoal) SOLID SORBENT TUBE (coconut shell charcoal, 400 mg/200 mg) SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg) SOLID SORBENT TUBE (carbon molecular sieve; 160 mg/80 mg; ORBO-92 or equivalent) SOLID SORBENT TUBE (silica gel, 150 mg/75 mg) FILTER (1-μm PTFE membrane) FILTER (0.8-μm cellulose ester membrane FILTER (0.8-μm PVC membrane, 25-mm diameter, in open-face cassette) CYCLONE + FILTER (10-mm cyclone or Higgins-Dewell (HD) + 5-μm PVC membrane)
FLOW RATE
MEASUREMENT TECHNIQUE
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 1.0 L/min
GAS CHROMATOGRAPHY, FID
0.05 to 0.2 L/min
ION CHROMATOGRAPHY, CONDUCTIVITY DETECTION
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.2 to 1.0 L/min
VISIBLE ABSORPTION SPECTROPHOTOMETRY
0.1 to 0.5 L/min
HPLC, UV
2 L/min
HPLC, FLUORESCENCE/UV DETECTION
0.5 to 2 L/min
GAS CHROMATOGRAPHY, FID
0.2 to 1 L/min
GC, FLAME PHOTOMETRIC DETE
0.3 to 1 L/min
ION CHROMATOGRAPHY, CONDUCTIVITY
0.1 to 0.2 L/min
VISIBLE ABSORPTION SPECTROPHOTOMETRY
0.01 to 0.05 L/min
GAS CHROMATOGRAPH, FID
0.01 to 0.05 L/min
GAS CHROMATOGRAPHY, FID
1 to 4 L/min
ATOMIC ABSORPTION, FLAME
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
1 to 3 L/min
GC, FPD with a phosphorus filter
HD cyclone: 2.2 L/min; nylon cyclone: 1.7 L/min
VISIBLE ABSORPTION SPECTROPHOTOMETRY
0.5 to 1.5 L/min
ION CHROMATOGRAPHY
0.05 to 0.1 L/min
ION CHROMATOGRAPHY CONDUCTIVITY DETECTION
1 to 2 L/min
FLOW INJECTION, FLUORESCENCE DETECTOR
1 to 3 L/min
ICP-AES OR AAS
0.1 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
HD cyclone: 2.2 L/min nylon cyclone: 1.7 L/min
GAS CHROMATOGRAPHY WITH ELECTROLYTIC CONDUCTIVITY DETECTOR (HALL) INFRARED ABSORPTION SPECTROPHOTOMETRY (IR)
0.1 to 1.5 L/min
HPLC; UV DETECTION
0.01 to 0.2 L/min
0.01 to 1 L/min
GAS CHROMATOGRAPHY, FID
0.2 to 1 L/min
VISIBLE ABSORPTION SPECTROPHOTOMETRY
0.01 to 0.1 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.01 - 0.2 L/min
UV-VIS SPECTROMETER
0.1 to 1 L/min
HPLC, UV detection
1 to 3 L/min
INFRARED SPECTROPHOTOMETRY
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, SULFURSPECIFIC FPD
0.01 to 0.05 L/min
THERMAL DESORPTION, GAS CHROMATOGRAPHY, MASS SPECTROMETRY
1 to 3 L/min
HPLC, UV DETECTION
LONG-PATHLENGTH PORTABLE INFRARED SPECTROPHOTOMETER (FIELD READOUT 0.2 to 2 L/min
GAS CHROMATOGRAPHY,
1.0 to 2.0 L/min
GAS CHROMATOGRAPHY, NITROGEN CHEMILUMINESCENCE DETECTOR
0.01 to 0.05 L/min
GAS CHROMATOGRAPHY, FLAME IONIZATION DETECTOR
0.01 to 0.05 L/min
GAS CHROMATOGRAPHY, NITROGENSPECIFIC DETECTOR
0.2 to 1.0 L/min
GAS CHROMATOGRAPHY, ECD
0.01 to 0.05 L/min
GAS CHROMATOGRAPHY, FLAME IONIZATION DETECTOR
0.2 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.02 L/min
GAS CHROMATOGRAPHY, FID
NO: 0.025 L/min NO2: 0.025 - 0.2 L/min
VISIBLE ABSORPTION SPECTROPHOTOMETRY
1.0 L/min
GAS CHROMATOGRAPHY-NITROGEN PHOSPHOROUS DETECTOR
0.05 to 0.2 L/min
ATOMIC ABSORPTION, GRAPHITE FURNACE
0.2 to 0.8 L/min
GAS CHROMATOGRAPHY, FID ANALYTE
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.1 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.5 to 2 L/min
VISIBLE ABSORPTION SPECTROPHOTOMETRY
0.5 to 1.5 L/min
VISIBLE SPECTROPHOTOMETRY
0.2 to 1.0 L/min
GAS CHROMATOGRAPHY, FID
0.25 to 1 L/min
GAS CHROMATOGRAPHY, FPD
0.01 to 1 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FI
0.01 to 0.1 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.1 L/min
GAS CHROMATOGRAPHY, ATOMIC EMISSION DETECTION (GC-AED) monitoring Br, C and H channels
0.01 to 0.05 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FI
0.02 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
HD cyclone: 2.2 L/min nylon cyclone: 1.7 L/min
X-RAY POWDER DIFFRACTION
1 to 4 L/min
INDUCTIVELY COUPLED ARGON PLASMA, ATOMIC EMISSION SPECTROSCOPY (ICP-AES)
1 to 4 L/min
ACID-BASE TITRATION
2 L/min
CHEMICAL SPOT TEST KIT (Rhodizonate-based)
1 to 4 L/min
ATOMIC ABSORPTION SPECTROPHOTOMETER, FLAME
0.5 to 1 L/min
GAS CHROMATOGRAPHY, ECD
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 1 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.05 L/min
GAS CHROMATOGRAPHY, FID
0.02 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
1 L/min
HPLC, ELECTROCHEMICAL AND UV DETECTION
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.05 to 0.2 L/min
GAS CHROMATOGRAPHY/ECD
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, 63Ni ECD
1 to 4 L/min
HPLC, UV DETECTION
0.1 to 1.5 L/min ION CHROMATOGRAPHY, -RECOMMENDED: 0.2 L/minCONDUCTIVITY
0.05 to 0.2 L/min
SPECTROPHOTOMETRY, VISIBLE ABSORPTION
0.2 to 1.0 L/min
SPECTROPHOTOMETRY, VISIBLE ABSORPTION
1 to 2 L/min
HPLC, FLUORESCENCE DETECTOR/ ELECTROCHEMICAL DETECTOR
1 to 2 L/min
HPLC, FLUORESCENCE DETECTOR/ ELECTROCHEMICAL DETECTOR
0.05 to 0.5 L/min
HPLC, UV DETECTION
0.01 to 0.10 L/min
GAS CHROMATOGRAPHY, FID
2 L/min
GAS CHROMATOGRAPHY, CAPILLARY COLUMN, FID
1 to 2 L/min
ION-SPECIFIC ELECTRODE
0.05 to 0.2 L/min
ION CHROMATOGRAPHY, CONDUCTIVITY DETECTION
0.03 to 1.5 L/min
HPLC, UV DETECTION
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.1 to 0.2 L/min
GAS CHROMATOGRAPHY
0.01 to 0.2 L/min
GAS CHROMOTOGRAPHY, FID
0.2 L/min
HPLC, UV DETECTION
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
GAS CHROMATOGRAPHY, FID
0.02 to 0.05 L/min
SOLID SORBENT TUBES (2 coconut shell charcoal tubes,
400 mg and 200 mg) 0.01 to 0.2 L/minute
GAS CHROMATOGRAPHY, FID
0.01 to 0.05 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
1 to 3 L/min
HPLC, UV DETECTION
0.01 to 0.05 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 1.0 L/min
GAS CHROMATOGRAPHY, FID
0.5 to 1 L/min
ION CHROMATOGRAPHY, ion pairing
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.2 L/min
GAS CHROMATOGRAPHY, FID
0.2 to 1 L/min
GAS CHROMATOGRAPHY/ ELECTRON CAPTURE DETECTOR (GC/ECD)
1 to 3 L/min
HPLC, UV DETECTION
1 to 4 L/min
VISIBLE ABSORPTION SPECTROPHOTOMETRY
0.2 to 0.5 L/min
ION CHROMATOGRAPHY
GAS CHROMATOGRAPHY, FID 0.01 to 0.2 L/min
1 to 3 L/mi
ATOMIC ABSORPTION, GRAPHITE FURNACE
0.05 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.01 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
0.1 to 0.2 L/min
GAS CHROMATOGRAPHY, FID
GAS CHROMATOGRAPHY, FID
1 to 4 L/min
HPLC, UV DETECTION
1 to 3 L/min
ATOMIC ABSORPTION, FLAME
1 to 3 L/min
X-RAY POWDER DIFFRACTION
HD cyclone: 2.2 L/min nylon cyclone: 1.7 L/min
X-RAY POWDER DIFFRACTION
TYPES OF CHEMICAL HYDROCARBON HALOGENATED
SOBRENT TYPES
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ALCOHOLS III
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ALCOHOLS COMBINED
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (Coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ACETIC ACID
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg)
0.01 to 1.0 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL CHLOROACETIC ACID
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (silica gel, 100 mg/50 mg)
0.05 to 0.2 L/min
MEASUREMENT TECHNIQUE ION CHROMATOGRAPHY, CONDUCTIVITY DETECTION
TYPES OF CHEMICAL KETONES I
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (Anasorb CMS, 150 mg/75 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ACETIC ANHYDRIDE
SAMPLING MEDIA
FLOW RATE
LIQUID IN BUBBLER (mixed bubbler with 10 mL alkaline hydroxylamine)
0.2 to 1.0 L/min
MEASUREMENT TECHNIQUE VISIBLE ABSORPTION SPECTROPHOTOMETRY
TYPES OF CHEMICAL ACETALDEHYDE by HPLC
SAMPLING MEDIA
FLOW RATE
LIQUID IN BUBBLER (midget bubbler containing 15 mL Girard T solution @ pH 4.5)
0.1 to 0.5 L/min
MEASUREMENT TECHNIQUE HPLC, UV
TYPES OF CHEMICAL POLYNUCLEAR AROMATIC HYDROCARBONS
SAMPLING MEDIA
FLOW RATE
FILTER + SORBENT TUBE (37-mm, 2-μm, PTFE + washed XAD-2, 100 mg/50 mg)
2 L/min
MEASUREMENT TECHNIQUE HPLC, FLUORESCENCE/UV DETECTION
TYPES OF CHEMICAL GLYCOLS
SAMPLING MEDIA
FLOW RATE
XAD-7 OVS tube (glass fiber filter, 13-mm; XAD-7, 200mg/100mg)
0.5 to 2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ORGANOPHOSPHORUS PESTICIDES
SAMPLING MEDIA
FLOW RATE
FILTER/SOLID SORBENT TUBE (OVS-2 tube: 13-mm quartz filter; XAD-2, 270 mg/140 mg
0.2 to 1 L/min
MEASUREMENT TECHNIQUE GC, FLAME PHOTOMETRIC DETE
TYPES OF CHEMICAL BROMINE
SAMPLING MEDIA
FLOW RATE
PREFILTER + FILTER (PTFE, 0.5-μm + silver membrane, 25-mm, 0.45-μm)
0.3 to 1 L/min
MEASUREMENT TECHNIQUE ION CHROMATOGRAPHY, CONDUCTIVITY
TYPES OF CHEMICAL AMMONIA
SAMPLING MEDIA SOLID SORBENT TUBE (sulfuric acid-treated silica gel) A 0.8-micron MCE prefilter may be used to remove particulate interferences.
FLOW RATE 0.1 to 0.2 L/min
MEASUREMENT TECHNIQUE VISIBLE ABSORPTION SPECTROPHOTOMETRY
TYPES OF CHEMICAL 1,1,2-TRICHLORO-1,2,2-TRIFLUOROETHANE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg
0.01 to 0.05 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPH, FID
TYPES OF CHEMICAL TRIFLUOROBROMOMETHANE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBES (two coconut shell charcoal tubes in series, 400 mg/200 mg and 100 mg/50 mg)
0.01 to 0.05 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL TUNGSTEN (soluble and insoluble)
SAMPLING MEDIA
FLOW RATE
FILTER (0.8-μm cellulose ester membrane
1 to 4 L/min
MEASUREMENT TECHNIQUE ATOMIC ABSORPTION, FLAME
TYPES OF CHEMICAL TRICHLOROETHYLENE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL TRIBUTYL PHOSPHATE
SAMPLING MEDIA
FLOW RATE
FILTER (0.8-μm mixed cellulose ester membrane); above 23 C, use two filter cassettes in series
1 to 3 L/min
MEASUREMENT TECHNIQUE GC, FPD with a phosphorus filter
TYPES OF CHEMICAL SILICA, CRYSTALLINE,
SAMPLING MEDIA
FLOW RATE
CYCLONE + FILTER (10-mm cyclone, nylon or HigginsDewell (HD) + 0.8-:m MCE or 5-:m PVC)
HD cyclone: 2.2 L/min; nylon cyclone: 1.7 L/min
MEASUREMENT TECHNIQUE VISIBLE ABSORPTION SPECTROPHOTOMETRY
TYPES OF CHEMICAL SULFUR DIOXIDE
SAMPLING MEDIA
FLOW RATE
FILTER + TREATED FILTER (cellulose + Na2CO3; preceded by 0.8-μm cellulose ester membrane)
0.5 to 1.5 L/min
MEASUREMENT TECHNIQUE ION CHROMATOGRAPHY
TYPES OF CHEMICAL SULFURYL FLUORIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 800 mg/200 mg)
0.05 to 0.1 L/min
MEASUREMENT TECHNIQUE ION CHROMATOGRAPHY CONDUCTIVITY DETECTION
TYPES OF CHEMICAL POLYCYCLIC AROMATIC COMPOUNDS, TOTAL (PACs
SAMPLING MEDIA
FLOW RATE
FILTER + SOLID SORBENT (2-μm, 37-mm, PTFE filter + washed XAD-2 resin, 100/50 mg )
1 to 2 L/min
MEASUREMENT TECHNIQUE FLOW INJECTION, FLUORESCENCE DETECTOR
TYPES OF CHEMICAL SUPER ABSORBENT POLYMERS
SAMPLING MEDIA
FLOW RATE
MEMBRANE FILTER (PVC, 5-μm, 37-mm)
1 to 3 L/min
MEASUREMENT TECHNIQUE ICP-AES OR AAS
TYPES OF CHEMICAL GLYCOL ETHERS
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (Anasorb® 747, 140 mg/70 mg)
0.1 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL PROPYLENE DICHLORIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (petroleum charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY WITH ELECTROLYTIC CONDUCTIVITY DETECTOR (HALL)
TYPES OF CHEMICAL QUARTZ in coal mine dust, by IR (redeposition)
SAMPLING MEDIA
FLOW RATE
CYCLONE + PREWEIGHED FILTER (10-mm cyclone, nylon or Higgins-Dewell (HD), and PVC filter, 37-mm, 5-μm)
HD cyclone: 2.2 L/min nylon cyclone: 1.7 L/min
MEASUREMENT TECHNIQUE INFRARED ABSORPTION SPECTROPHOTOMETRY (IR)
TYPES OF CHEMICAL ALIPHATIC ALDEHYDES
SAMPLING MEDIA
FLOW RATE
CARTRIDGE (containing silica gel coated with acidified 2,4dinitrophenylhydrazine)
0.1 to 1.5 L/min
MEASUREMENT TECHNIQUE HPLC; UV DETECTION
TYPES OF CHEMICAL PHENYL GLYCIDYL ETHER
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal; 100 mg/50 mg)
0.01 to 1 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL PHENYLHYDRAZINE
SAMPLING MEDIA
FLOW RATE
GLASS MIDGET BUBBLER (containing 15 mL 0.1 M hydrochloric acid)
0.2 to 1 L/min
MEASUREMENT TECHNIQUE VISIBLE ABSORPTION SPECTROPHOTOMETRY
TYPES OF CHEMICAL CRESOL (all isomers) and PHENOL
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (XAD-7, 100 mg/50 mg)
0.01 to 0.1 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL PHENYL ETHER
SAMPLING MEDIA
FLOW RATE
CHARCOAL TUBE (coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL PHOSPHINE
SAMPLING MEDIA
FLOW RATE
SORBENT TUBE (Hg(CN)2-coated silica gel, 300 mg/150 mg)
0.01 - 0.2 L/min
MEASUREMENT TECHNIQUE UV-VIS SPECTROMETER
TYPES OF CHEMICAL ORGANONITROGEN PESTICIDES
SAMPLING MEDIA
FLOW RATE
FILTER/SOLID SORBENT TUBE (OVS-2 Tube: 13-mm quartz fiber filter; XAD-2, 270 mg/140 mg)
0.1 to 1 L/min
MEASUREMENT TECHNIQUE HPLC, UV detection
TYPES OF CHEMICAL OIL MIST, MINERAL
SAMPLING MEDIA
FLOW RATE
MEMBRANE FILTER (37-mm diameter, 0.8-:m MCE, 5-:m PVC, 2-:m PTFE, or glass fiber)
1 to 3 L/min
MEASUREMENT TECHNIQUE INFRARED SPECTROPHOTOMETRY
TYPES OF CHEMICAL 1-OCTANETHIOL
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (Tenax-GC, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, SULFURSPECIFIC FPD
TYPES OF CHEMICAL VOLATILE ORGANIC COMPOUNDS
SAMPLING MEDIA
FLOW RATE
THERMAL DESORPTION TUBE TECHNIQUE (multi-bed sorbent tubes containing graphitized carbons and carbon molecular sieve sorbents
0.01 to 0.05 L/min
MEASUREMENT TECHNIQUE THERMAL DESORPTION, GAS CHROMATOGRAPHY, MASS SPECTROMETRY
TYPES OF CHEMICAL p-NITROANILINE
SAMPLING MEDIA
FLOW RATE
FILTER (0.8 μm mixed cellulose ester membrane
1 to 3 L/min
MEASUREMENT TECHNIQUE HPLC, UV DETECTION
TYPES OF CHEMICAL NITROUS OXIDE
SAMPLING MEDIA AMBIENT AIR OR BAG SAMPLE
FLOW RATE
MEASUREMENT TECHNIQUE LONG-PATHLENGTH PORTABLE INFRARED SPECTROPHOTOMETER (FIELD READOUT
TYPES OF CHEMICAL NITROSAMINES
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (Thermosorb/N™ air sampler
0.2 to 2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY,
TYPES OF CHEMICAL 1-NITROPYRENE IN DIESEL PARTICULATES
SAMPLING MEDIA
FLOW RATE
FILTER (Glass Fiber, 37-mm)
1.0 to 2.0 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, NITROGEN CHEMILUMINESCENCE DETECTOR
TYPES OF CHEMICAL 2-NITROPROPANE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (Chromosorb 106, 100 mg/50 mg)
0.01 to 0.05 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FLAME IONIZATION DETECTOR
TYPES OF CHEMICAL NITROMETHANE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (Chromosorb 106, 600 mg/300 mg)
0.01 to 0.05 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, NITROGENSPECIFIC DETECTOR
TYPES OF CHEMICAL NITROGLYCERIN
SAMPLING MEDIA
FLOW RATE
SOLID SAMPLER TUBE (Tenax-GC, 100 mg/50 mg)
0.2 to 1.0 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, ECD
TYPES OF CHEMICAL NITROETHANE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBES (XAD-2, 600 mg + 300 mg)
0.01 to 0.05 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FLAME IONIZATION DETECTOR
TYPES OF CHEMICAL ANILINE, o-TOLUIDINE, AND NITROBENZENE
SAMPLING MEDIA
FLOW RATE
FILTER + SOLID SORBENT (Glass fiber filter, sulfuric acid treated + silica gel sorbent tube, 520/260 mg)
0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL NITROAROMATIC COMPOUNDS
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (Silica gel, 150 mg/75 mg)
0.01 to 0.02 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL NITRIC OXIDE and NITROGEN DIOXIDE
SAMPLING MEDIA
FLOW RATE
SORBENT TUBES (oxidizer + 2 triethanolamine-treated molecular sieve)
NO: 0.025 L/min NO2: 0.025 - 0.2 L/min
MEASUREMENT TECHNIQUE VISIBLE ABSORPTION SPECTROPHOTOMETRY
TYPES OF CHEMICAL NICOTINE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE XAD-2 (100 mg/50 mg)
1.0 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY-NITROGEN PHOSPHOROUS DETECTOR
TYPES OF CHEMICAL NICKEL CARBONYL
SAMPLING MEDIA
FLOW RATE
PREFILTER + SOLID SORBENT TUBE (low-Ni charcoal, 120 mg/60 mg; 0.8-μm cellulose ester membrane
0.05 to 0.2 L/min
MEASUREMENT TECHNIQUE ATOMIC ABSORPTION, GRAPHITE FURNACE
TYPES OF CHEMICAL NAPHTHYLAMINES, a and b
SAMPLING MEDIA
FLOW RATE
FILTER + SOLID SORBENT (glass fiber + silica gel, 100 mg/50 mg)
0.2 to 0.8 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID ANALYTE
TYPES OF CHEMICAL NAPHTHAS
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL METHYL tert-BUTYL ETHER
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBES (two charcoal tubes in series; front 400 mg; back 200 mg)
0.1 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL METHYL ETHYL KETONE PEROXIDE
SAMPLING MEDIA
FLOW RATE
IMPINGER (15 mL dimethyl phthalate)
0.5 to 2 L/min
MEASUREMENT TECHNIQUE VISIBLE ABSORPTION SPECTROPHOTOMETRY
TYPES OF CHEMICAL MONOMETHYLHYDRAZINE
SAMPLING MEDIA
FLOW RATE
BUBBLER (0.1 M hydrochloric acid)
0.5 to 1.5 L/min
MEASUREMENT TECHNIQUE VISIBLE SPECTROPHOTOMETRY
TYPES OF CHEMICAL MONOMETHYLANILINE
SAMPLING MEDIA
FLOW RATE
MIDGET BUBBLER (0.05 M sulfuric acid, 10 mL)
0.2 to 1.0 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL METHYLTIN CHLORIDES
SAMPLING MEDIA
FLOW RATE
FILTER + SORBENT TUBE (OVS Tube: 13-mm glass fiber filter; XAD-2, 270/140 mg)
0.25 to 1 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FPD
TYPES OF CHEMICAL METHYL IODIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg)
0.01 to 1 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL METHYL ETHYL KETON
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (beaded carbon, ~150 mg/~75 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FI
TYPES OF CHEMICAL METHYL CHLORIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBES (two coconut shell charcoal tubes in series, 400 mg/200 mg and 100 mg/50 mg)
0.01 to 0.1 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL METHYL BROMIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBES (two petroleum charcoal tubes, 400 mg and 200 mg; drying tube, 9-g Na2SO4, necessary at humidity >50%)
0.01 to 0.1 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, ATOMIC EMISSION DETECTION (GC-AED) monitoring Br, C and H channels
TYPES OF CHEMICAL METHYL AND ETHYL METHACRYLATE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (XAD-2, 400/200 mg)
0.01 to 0.05 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL METHYL CELLOSOLVE ACETATE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FI
TYPES OF CHEMICAL METHANOL
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (silica gel, 100/50 mg)
0.02 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL LEAD SULFIDE
SAMPLING MEDIA
FLOW RATE
CYCLONE + FILTER (10-mm nylon or Higgins-Dewell (HD) cyclone
HD cyclone: 2.2 L/min nylon cyclone: 1.7 L/min
MEASUREMENT TECHNIQUE X-RAY POWDER DIFFRACTION
TYPES OF CHEMICAL ELEMENTS by ICP 7301 (Aqua Regia Ashing) antimony* chromium* lithium potassium tin zirconium* arsenic cobalt magnesium selenium titanium barium copper manganese silver tungsten* beryllium iron* molybdenum strontium vanadium cadmium lanthanum nickel tellurium yttrium
SAMPLING MEDIA
FLOW RATE
FILTER (0.8-μm, cellulose ester membrane, or 5.0-μm, polyvinyl chloride membrane
1 to 4 L/min
MEASUREMENT TECHNIQUE INDUCTIVELY COUPLED ARGON PLASMA, ATOMIC EMISSION SPECTROSCOPY (ICP-AES)
TYPES OF CHEMICAL ALKALINE DUSTS
SAMPLING MEDIA
FLOW RATE
FILTER (1-μm PTFE membrane)
1 to 4 L/min
MEASUREMENT TECHNIQUE ACID-BASE TITRATION
TYPES OF CHEMICAL LEAD in Air by Chemical Spot Test
SAMPLING MEDIA
FLOW RATE
FILTER (0.8-μm cellulose ester membrane)
2 L/min
MEASUREMENT TECHNIQUE CHEMICAL SPOT TEST KIT (Rhodizonate-based)
TYPES OF CHEMICAL LEAD by Flame AAS
SAMPLING MEDIA
FLOW RATE
FILTER (0.8-μm cellulose ester membrane
1 to 4 L/min
MEASUREMENT TECHNIQUE ATOMIC ABSORPTION SPECTROPHOTOMETER, FLAME
TYPES OF CHEMICAL KEPONE
SAMPLING MEDIA
FLOW RATE
FILTER + IMPINGER (0.8-μm cellulose ester membrane + impinger with 0.1 M NaOH)
0.5 to 1 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, ECD
TYPES OF CHEMICAL NAPHTHAS
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ISOPHORONE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (petroleum-based charcoal,
0.01 to 1 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ISOPROPYL ETHER
SAMPLING MEDIA
FLOW RATE
Solid Sorbent Tube (coconut shell charcoal; 100 mg/50 mg)
0.01 to 0.05 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ISOPROPYL ACETATE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg,
0.02 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ISOCYANATES, MONOMERIC
SAMPLING MEDIA
FLOW RATE
IMPINGER (solution of 1-(2-methoxyphenyl)-piperazine in toluene)
1 L/min
MEASUREMENT TECHNIQUE HPLC, ELECTROCHEMICAL AND UV DETECTION
TYPES OF CHEMICAL ALCOHOLS II
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL HEXACHLOROBUTADIENE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (XAD-2; 100 mg/50 mg)
0.05 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY/ECD
TYPES OF CHEMICAL HEXACHLORO-1,3-CYCLOPENTADIENE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (2 tubes, Porapak T, 75 mg and 25 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, 63Ni ECD
TYPES OF CHEMICAL HYDROQUINONE
SAMPLING MEDIA
FLOW RATE
FILTER (0.8-μm cellulose ester membrane
1 to 4 L/min
MEASUREMENT TECHNIQUE HPLC, UV DETECTION
TYPES OF CHEMICAL HYDROGEN SULFIDE
SAMPLING MEDIA
FLOW RATE
FILTER + SOLID SORBENT TUBE (Zefluor, 0.5 μm; coconut shell charcoal, 400 mg/200 mg
0.1 to 1.5 L/min -RECOMMENDED: 0.2 L/min
MEASUREMENT TECHNIQUE ION CHROMATOGRAPHY, CONDUCTIVITY
TYPES OF CHEMICAL HYDROGEN CYANIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (soda lime, 600 mg/200 mg)
0.05 to 0.2 L/min
MEASUREMENT TECHNIQUE SPECTROPHOTOMETRY, VISIBLE ABSORPTION
TYPES OF CHEMICAL HYDRAZINE
SAMPLING MEDIA
FLOW RATE
BUBBLER (15 mL 0.1 M HCl)
0.2 to 1.0 L/min
MEASUREMENT TECHNIQUE SPECTROPHOTOMETRY, VISIBLE ABSORPTION
TYPES OF CHEMICAL ISOCYANATES
SAMPLING MEDIA
FLOW RATE
IMPINGER (tryptamine/DMSO; 20 mL)
1 to 2 L/min
MEASUREMENT TECHNIQUE HPLC, FLUORESCENCE DETECTOR/ ELECTROCHEMICAL DETECTOR
TYPES OF CHEMICAL GLUTARALDEHYDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE 0.05 to 0.5 L/min (silica gel coated with 2,4-dinitrophenylhydrazine HCl, 300 mg/150 mg
MEASUREMENT TECHNIQUE HPLC, UV DETECTION
TYPES OF CHEMICAL FORMALDEHYDE by GC
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (10% (2-hydroxymethyl)piperdine on XAD-2, 120 mg/60 mg
0.01 to 0.10 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL POLYNUCLEAR AROMATIC HYDROCARBONS
SAMPLING MEDIA
FLOW RATE
FILTER + SORBENT (2-μm, 37-mm PTFE + washed XAD-2, 100 mg/50 mg)
2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, CAPILLARY COLUMN, FID
TYPES OF CHEMICAL FLUORIDES, aerosol and gas
SAMPLING MEDIA
FLOW RATE
FILTER + TREATED PAD (0.8-μm cellulose ester membrane + Na2CO3-treated cellulose pad)
1 to 2 L/min
MEASUREMENT TECHNIQUE ION-SPECIFIC ELECTRODE
TYPES OF CHEMICAL FORMIC ACID
SAMPLING MEDIA
FLOW RATE
FILTER + SOLID SORBENT TUBE (PTFE membrane, 5-μm + washed, silica gel, 400 mg/200 mg)
0.05 to 0.2 L/min
MEASUREMENT TECHNIQUE ION CHROMATOGRAPHY, CONDUCTIVITY DETECTION
TYPES OF CHEMICAL FORMALDEHYDE
SAMPLING MEDIA
FLOW RATE
CARTRIDGE (Cartridge containing silica gel coated with 2,4-dinitrophenylhydrazine)
0.03 to 1.5 L/min
MEASUREMENT TECHNIQUE HPLC, UV DETECTION
TYPES OF CHEMICAL PROPYLENE OXIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ETHYL BROMIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL MERCAPTANS, METHYL-, ETHYL-, and n-BUTYL
SAMPLING MEDIA
FLOW RATE
FILTER (glass fiber, 37-mm, impregnated with mercuric acetate)
0.1 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY
TYPES OF CHEMICAL ETHYL ETHER
SAMPLING MEDIA
FLOW RATE
Solid Sorbent Tube (coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMOTOGRAPHY, FID
TYPES OF CHEMICAL ETHYLENIMINE
SAMPLING MEDIA
FLOW RATE
BUBBLER (Folin's reagent
0.2 L/min
MEASUREMENT TECHNIQUE HPLC, UV DETECTION
TYPES OF CHEMICAL ESTERS 1
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ETHYLENE CHLOROHYDRIN
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (petroleum charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL HYDROCARBONS, AROMATIC
SAMPLING MEDIA SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg)
FLOW RATE
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ETHYL CHLORIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBES (2 coconut shell charcoal tubes, 400 mg and 200 mg)
0.02 to 0.05 L/min
MEASUREMENT TECHNIQUE SOLID SORBENT TUBES (2 coconut shell charcoal tubes, 400 mg and 200 mg)
TYPES OF CHEMICAL ETHYL ACETATE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.2 L/minute
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ALCOHOLS IV
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (Coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.05 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL AMINOETHANOL COMPOUNDS I
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (silica gel, 300 mg/150 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL DYES, BENZIDINE-, o-TOLIDINE-, o-DIANISIDINE
SAMPLING MEDIA
FLOW RATE
FILTER (5-μm PTFE membrane
1 to 3 L/min
MEASUREMENT TECHNIQUE HPLC, UV DETECTION
TYPES OF CHEMICAL DICHLOROFLUOROMETHANE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBES (2 coconut shell charcoal tubes, 400 mg and 200 mg)
0.01 to 0.05 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL AMINES, ALIPHATIC
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (silica gel, 150 mg / 75 mg)
0.01 to 1.0 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL AMINOETHANOL COMPOUNDS II
SAMPLING MEDIA
FLOW RATE
IMPINGER (15 mL 2 mM hexanesulfonic acid)
0.5 to 1 L/min
MEASUREMENT TECHNIQUE ION CHROMATOGRAPHY, ion pairing
TYPES OF CHEMICAL METHYLENE CHLORIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT (2 coconut shell charcoal tubes, 100/50 mg
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL DIAZOMETHANE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (octanoic acid-coated XAD-2 resin, 100 mg/50 mg)
0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL CHLORINATED AND ORGANONITROGEN HERBICIDES
SAMPLING MEDIA
FLOW RATE
FILTER/SOLID SORBENT TUBE (OVS tube: 11-mm quartz filter; XAD-2)
0.2 to 1 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY/ ELECTRON CAPTURE DETECTOR (GC/ECD)
TYPES OF CHEMICAL 2,4-D
SAMPLING MEDIA
FLOW RATE
FILTER (glass fiber, binderless
1 to 3 L/min
MEASUREMENT TECHNIQUE HPLC, UV DETECTION
TYPES OF CHEMICAL CHROMIUM, HEXAVALENT
SAMPLING MEDIA
FLOW RATE
FILTER (5.0-μm PVC membrane)
1 to 4 L/min
MEASUREMENT TECHNIQUE VISIBLE ABSORPTION SPECTROPHOTOMETRY
TYPES OF CHEMICAL ACIDS, INORGANIC
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (washed silica gel, 400 mg/200 mg with glass fiber filter plug)
0.2 to 0.5 L/min
MEASUREMENT TECHNIQUE ION CHROMATOGRAPHY
TYPES OF CHEMICAL ACETONITRILE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 400/200 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL ARSENIC TRIOXIDE
SAMPLING MEDIA FILTER (Na2CO3-impregnated, 0.8-μm cellulose ester membrane + backup pad)
FLOW RATE
MEASUREMENT TECHNIQUE
1 to 3 L/mi
ATOMIC ABSORPTION, GRAPHITE FURNACE
TYPES OF CHEMICAL VANADIUM OXIDES
SAMPLING MEDIA
FLOW RATE
CYCLONE + FILTER (10-mm cyclone or Higgins-Dewell (HD) + 5-μm PVC membrane)
HD cyclone: 2.2 L/min nylon cyclone: 1.7 L/min
MEASUREMENT TECHNIQUE X-RAY POWDER DIFFRACTION
TYPES OF CHEMICAL ZINC OXIDE
SAMPLING MEDIA
FLOW RATE
FILTER (0.8-μm PVC membrane, 25-mm diameter, in open-face cassette)
1 to 3 L/min
MEASUREMENT TECHNIQUE X-RAY POWDER DIFFRACTION
TYPES OF CHEMICAL ZINC and compounds, as Zn
SAMPLING MEDIA
FLOW RATE
FILTER (0.8-μm cellulose ester membrane
1 to 3 L/min
MEASUREMENT TECHNIQUE ATOMIC ABSORPTION, FLAME
TYPES OF CHEMICAL WARFARIN
SAMPLING MEDIA
FLOW RATE
FILTER (1-μm PTFE membrane)
1 to 4 L/min
MEASUREMENT TECHNIQUE HPLC, UV DETECTION
TYPES OF CHEMICAL AMINES, AROMATIC
SAMPLING MEDIA SOLID SORBENT TUBE (silica gel, 150 mg/75 mg)
FLOW RATE
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL VINYL ACETATE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (carbon molecular sieve; 160 mg/80 mg; ORBO-92 or equivalent)
0.1 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL VINYLIDENE CHLORIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 100 mg/50 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL VINYL BROMIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (coconut shell charcoal, 400 mg/200 mg)
0.01 to 0.2 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
TYPES OF CHEMICAL VINYL CHLORIDE
SAMPLING MEDIA
FLOW RATE
SOLID SORBENT TUBE (2 tandem tubes, each with 150 mg activated coconut charcoal)
0.05 L/min
MEASUREMENT TECHNIQUE GAS CHROMATOGRAPHY, FID
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