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Fig (23) Spectra of the compound (49-e) pH Absorbance [λ=305 nm] 3 1.720 4 1.670 5 1.455 6 1.282 7 1.219 8 1.199 9 1.190 10 1.182 11 1.180 Fig (25) Spectra of the compound (49-g) pH Absorbance Absorbance [λ=314 nm] [λ=378 nm] 3 1.881 0.055 4 1.826 0.125 5 1.480 0.386 6 0.960 0.751 7 0.840 0.898 8 0.800 0.922 9 0.800 0.928 10 0.770 0.930 11 0.760 0.931 Fig (19) Spectra of the compound (49-a) pH Absorbance Absorbance [λ=315 nm] [λ=374 nm] 3 1.599 0.100 4 1.509 0.180 5 1.190 0.550 6 0.800 1.070 7 0.650 1.250 8 0.650 1.311 9 0.610 1.308 10 0.560 1.310 11 0.560 1.311
Fig (22) Spectra of the compound (49-d) pH Absorbance Absorbance [λ=260 nm] [λ=305 nm] 3 1.280 1.854 4 1.390 1.723 5 1.600 1.400 6 1.856 1.250 7 1.856 1.140 8 1.858 1.100 9 1.846 1.080 10 1.876 1.080 11 1.874 1.081 Fig (21) Spectra of the compound (49-c) pH Absorbance Absorbance [λ=280 nm] [λ=305 nm] 3 0.900 1.269 4 0.970 1.130 5 1.060 0.930 6 1.250 0.740 7 1.290 0.710 8 1.280 0.720 9 1.290 0.770 10 1.300 0.770 11 1.310 0.770 Fig (24) Spectra of the compound (49-f) pH Absorbance Absorbance [λ=280 nm] [λ=318 nm] 3 1.040 0.220 4 1.140 0.400 5 1.290 1.000 6 1.440 1.460 7 1.450 1.480 8 1.530 1.537 9 1.533 1.514 10 1.600 1.510 11 1.666 1.556
Fig (20) Spectra of the compound (49-b) pH Absorbance Absorbance [λ=266 nm] [λ=311 nm] 3 0.790 1.435 4 0.910 1.390 5 1.120 0.955 6 1.240 0.766 7 1.250 0.728 8 1.300 0.735 9 1.330 0.732 10 1.452 0.698 11 1.450 0.676 Fig (33) Spectra of Hf- (49-a) Cppm 500 400 300 200 100 50 25 10 5
Absorbance [λ=327 nm] 3.3 2.65 1.98 1.31 0.638 0.319 0.16 0.064 0.031
F 151 151 151 152 156.7 156.7 156 156 161
Fig (34) Spectra of Hf- (49-f) Cppm Absorbance F [λ=329 nm] 500 3.50 143 400 2.82 142 300 2.14 140 200 1.415 141 100 0.692 144.5 50 0.34 147 25 0.158 10 0.076 5 Out of scale
Fig (35) Spectra of Hf- (49-g) Cppm Absorbance F [λ=329 nm] 500 3.7 135 400 3.05 131 300 2.27 132 200 1.49 134 100 0.735 136 50 0.355 140 25 0.18 138 10 0.07 143 5 Out of scale Fig (36) Spectra of Hf- (49-b) Cppm Absorbance F [λ=322 nm] 500 2.95 169.5 400 2.37 168.8 300 1.806 166.1 200 1.215 164.6 100 0.925 162.16 50 0.615 162.6 25 0.474 158.23 10 0.318 157.23 5 0.15 166.67
Fig (37) Spectra of Hf- (49-e) Cppm Absorbance F [λ=343 nm] 1000 1.9 526 900 1.67 539 800 1.43 559 600 1.085 553 500 0.911 549 400 0.737 543 300 0.565 531 200 0.39 513 100 0.195 512 50 0.095 526 25 0.047 531 10 0.019 526 5 Out of scale Fig (38) Spectra of Zr- (49-a) Cppm Absorbance F [λ=384 nm] 1000 0.55 1818 900 0.495 1818 800 0.425 1882 600 0.313 1916 500 0.261 1915 400 0.212 1886 300 0.159 1886 200 0.113 1770 100 0.06 50 0.074 25 0.031 10 0.023
Fig (39) Spectra of Zr- (49-a) Cppm Absorbance F [λ=415 nm] 1000 0.225 900 0.195 800 0.174 600 0.135 500 0.118 400 0.1 300 0.085 200 0.056 100 0.048 50 0.038 25 0.032 10 0.026 Fig (40) Spectra of Zr- (49-f) Cppm Absorbance F [λ=417 nm] 1000 0.555 1801 900 0.5 1800 800 0.427 1873 600 0.322 1863 500 0.264 1894 400 0.212 1887 300 0.159 1887 200 0.111 1802 100 0.063 50 0.042 25 0.032 10 0.023
Fig (41) Spectra of Zr- (49-f) Cppm Absorbance F [λ=389 nm] 1000 1.58 633 900 1.426 631 800 1.121 661 600 0.9 666 500 0.733 682 400 0.587 681 300 0.44 682 200 0.301 664 100 0.16 625 50 0.095 25 0.062 10 0.044 Fig (42) Spectra of Zr- (49-g) Cppm Absorbance F [λ=433 nm] 1000 0.24 4166 900 0.204 4411 800 0.178 4494 600 0.135 4444 500 0.116 4310 400 0.079 4124 300 0.077 3896 200 0.062 3226 100 0.04 2500 50 0.03 25 0.025 10 0.022
Fig (43) Spectra of Zr- (49-g) Cppm Absorbance F [λ=392 nm] 1000 0.542 1845 900 0.484 1859 800 0.413 1937 600 0.309 1941 500 0.257 1945 400 0.204 1960 300 0.161 1863 200 0.118 100 0.084 50 0.069 25 0.044 10 0.033 Fig (44) Spectra of Zr- (49-b) Cppm Absorbance F [λ=417 nm] 1000 0.07 1429 900 0.505 1782 800 0.413 1937 600 0.294 2040 500 0.244 2049 400 0.186 2150 300 0.141 2127 200 0.098 2141 100 0.056 50 0.038 25 0.028 10 0.021
Fig (45) Spectra of Zr- (49-b) Cppm Absorbance F [λ=395 nm] 1000 1.37 730 900 1.095 822 800 0.894 894 600 0.648 926 500 0.528 947 400 0.410 975 300 0.303 990 200 0.206 971 100 0.112 893 50 0.069 25 0.047 10 0.032 Fig (46) Spectra of Zr- (49-e) Cppm Absorbance F [λ=410 nm] 1000 0.35 2857 900 0.315 2857 800 0.278 2877 600 0.21 2857 500 0.18 2778 400 0.145 2758 300 0.113 2655 200 0.102 100 0.076 50 0.05 25 0.035 10 0.23
Fig (47) Spectra of Zr- (49-e) Cppm Absorbance F [λ=383 nm] 1000 1.02 980 900 0.9 1000 800 0.783 1021 600 0.594 1010 500 0.505 990 400 0.4 1000 300 0.303 990 200 0.21 952 100 0.162 50 0.095 25 0.063 10 0.038
Fig (22) Spectra of the compound (49-d) pH Absorbance Absorbance [λ=260 nm] [λ=305 nm] 3 1.280 1.854 4 1.390 1.723 5 1.600 1.400 6 1.856 1.250 7 1.856 1.140 8 1.858 1.100 9 1.846 1.080 10 1.876 1.080 11 1.874 1.081 Fig (21) Spectra of the compound (49-c) pH Absorbance Absorbance [λ=280 nm] [λ=305 nm] 3 0.900 1.269 4 0.970 1.130 5 1.060 0.930 6 1.250 0.740 7 1.290 0.710 8 1.280 0.720 9 1.290 0.770 10 1.300 0.770 11 1.310 0.770 Fig (24) Spectra of the compound (49-f) pH Absorbance Absorbance [λ=280 nm] [λ=318 nm] 3 1.040 0.220 4 1.140 0.400 5 1.290 1.000 6 1.440 1.460 7 1.450 1.480 8 1.530 1.537 9 1.533 1.514 10 1.600 1.510 11 1.666 1.556
Fig (20) Spectra of the compound (49-b) pH Absorbance Absorbance [λ=266 nm] [λ=311 nm] 3 0.790 1.435 4 0.910 1.390 5 1.120 0.955 6 1.240 0.766 7 1.250 0.728 8 1.300 0.735 9 1.330 0.732 10 1.452 0.698 11 1.450 0.676 Fig (33) Spectra of Hf- (49-a) Cppm 500 400 300 200 100 50 25 10 5
Absorbance [λ=327 nm] 3.3 2.65 1.98 1.31 0.638 0.319 0.16 0.064 0.031
F 151 151 151 152 156.7 156.7 156 156 161
Fig (34) Spectra of Hf- (49-f) Cppm Absorbance F [λ=329 nm] 500 3.50 143 400 2.82 142 300 2.14 140 200 1.415 141 100 0.692 144.5 50 0.34 147 25 0.158 10 0.076 5 Out of scale
Fig (35) Spectra of Hf- (49-g) Cppm Absorbance F [λ=329 nm] 500 3.7 135 400 3.05 131 300 2.27 132 200 1.49 134 100 0.735 136 50 0.355 140 25 0.18 138 10 0.07 143 5 Out of scale Fig (36) Spectra of Hf- (49-b) Cppm Absorbance F [λ=322 nm] 500 2.95 169.5 400 2.37 168.8 300 1.806 166.1 200 1.215 164.6 100 0.925 162.16 50 0.615 162.6 25 0.474 158.23 10 0.318 157.23 5 0.15 166.67
Fig (37) Spectra of Hf- (49-e) Cppm Absorbance F [λ=343 nm] 1000 1.9 526 900 1.67 539 800 1.43 559 600 1.085 553 500 0.911 549 400 0.737 543 300 0.565 531 200 0.39 513 100 0.195 512 50 0.095 526 25 0.047 531 10 0.019 526 5 Out of scale Fig (38) Spectra of Zr- (49-a) Cppm Absorbance F [λ=384 nm] 1000 0.55 1818 900 0.495 1818 800 0.425 1882 600 0.313 1916 500 0.261 1915 400 0.212 1886 300 0.159 1886 200 0.113 1770 100 0.06 50 0.074 25 0.031 10 0.023
Fig (39) Spectra of Zr- (49-a) Cppm Absorbance F [λ=415 nm] 1000 0.225 900 0.195 800 0.174 600 0.135 500 0.118 400 0.1 300 0.085 200 0.056 100 0.048 50 0.038 25 0.032 10 0.026 Fig (40) Spectra of Zr- (49-f) Cppm Absorbance F [λ=417 nm] 1000 0.555 1801 900 0.5 1800 800 0.427 1873 600 0.322 1863 500 0.264 1894 400 0.212 1887 300 0.159 1887 200 0.111 1802 100 0.063 50 0.042 25 0.032 10 0.023
Fig (41) Spectra of Zr- (49-f) Cppm Absorbance F [λ=389 nm] 1000 1.58 633 900 1.426 631 800 1.121 661 600 0.9 666 500 0.733 682 400 0.587 681 300 0.44 682 200 0.301 664 100 0.16 625 50 0.095 25 0.062 10 0.044 Fig (42) Spectra of Zr- (49-g) Cppm Absorbance F [λ=433 nm] 1000 0.24 4166 900 0.204 4411 800 0.178 4494 600 0.135 4444 500 0.116 4310 400 0.079 4124 300 0.077 3896 200 0.062 3226 100 0.04 2500 50 0.03 25 0.025 10 0.022
Fig (43) Spectra of Zr- (49-g) Cppm Absorbance F [λ=392 nm] 1000 0.542 1845 900 0.484 1859 800 0.413 1937 600 0.309 1941 500 0.257 1945 400 0.204 1960 300 0.161 1863 200 0.118 100 0.084 50 0.069 25 0.044 10 0.033 Fig (44) Spectra of Zr- (49-b) Cppm Absorbance F [λ=417 nm] 1000 0.07 1429 900 0.505 1782 800 0.413 1937 600 0.294 2040 500 0.244 2049 400 0.186 2150 300 0.141 2127 200 0.098 2141 100 0.056 50 0.038 25 0.028 10 0.021
Fig (45) Spectra of Zr- (49-b) Cppm Absorbance F [λ=395 nm] 1000 1.37 730 900 1.095 822 800 0.894 894 600 0.648 926 500 0.528 947 400 0.410 975 300 0.303 990 200 0.206 971 100 0.112 893 50 0.069 25 0.047 10 0.032 Fig (46) Spectra of Zr- (49-e) Cppm Absorbance F [λ=410 nm] 1000 0.35 2857 900 0.315 2857 800 0.278 2877 600 0.21 2857 500 0.18 2778 400 0.145 2758 300 0.113 2655 200 0.102 100 0.076 50 0.05 25 0.035 10 0.23
Fig (47) Spectra of Zr- (49-e) Cppm Absorbance F [λ=383 nm] 1000 1.02 980 900 0.9 1000 800 0.783 1021 600 0.594 1010 500 0.505 990 400 0.4 1000 300 0.303 990 200 0.21 952 100 0.162 50 0.095 25 0.063 10 0.038
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