Experiment # 5

  • June 2020
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Maria Mota Experiment # 5 Sarah Zigmont The Preparation and Identification of an Unknown Ester References: Chemistry 320 B, laboratory manual, fall 2006, Berryhill, etal. Microscale and Macroscale Techniques in Organic Laboratory, 2002, Pavia etal. Chemfinder.com, 2004, CambridgeSoft Corporation. Balanced equation: Results:

Table # 1: IR analysis for alcohol # Frequency ppm

Bond Responsible

Table # 2: IR analysis for unknown ester Frequency ppm

Bond Responsible

Table # 1: NMR Analysis for Chemical Shift ppm Splitting Pattern/ Integration/ Adjacent proton Assignment

Table # 3: C NMR Chemical Shift ppm

Splitting Pattern

Assignment

Which Proton(s)

Which Proton

Discussion:

Questions:

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