Sabunnnnnnnnnnn.docx
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- Words: 868
- Pages: 6
F. Tools and Materials a. Tools 1. Beaker glass
1 piece
2. Spatula
1 piece
3. Pipette
10 piece
4. Stirring Rod
1 piece
5. Reflux condenser
1 piece
6. Funnel
1 piece
7. Separate Funnel
1 piece
8. Measuring glass
1 piece
9. Rounded bottom flask
1 piece
10. Erlenmeyer
1 piece
11. Clamps and statif
1 piece
12. Stem stirrer
1 piece
13. Filter paper
1 piece
14. Distillation condenser
1 piece
15. Thermometer
1 piece
16. Buret
1 piece
17. Ohaus balance sheet
1 piece
18. Tripod
1 piece
19. Rack
1 piece
20. Bunsen
1 piece
b. Materials 1. Coconut oil
22 grams
2. palm oil
22 gram
3. Bulk oil
22 grams
4. Ethanol
12 gram
5. NaOH
4.2 grams
6. Glycerin
12 grams
7. Olive oil
3 mL
8. Indicator PP
9 drops
9. Stearic acid
3 gram
10. Alcoholic KOH solution 0.1N
75 mL
11. Standard solution of 0.5 N HCl
30 mL
12. Dye
until enough
13. perfume
until enough
14. Aquades
until enough
G. LINES WORK 1. Soap Making 1,4 grams of NaOH 1. Disolved in 3,3 mL of water 2. Let it cool
NaOH solution
10 grams of Palm oil Add 1 gram of stearic acid stearic acid 2. Heat until 70°C until all all of of stearic acid melts 1.
Brownish mixture 3. 4. 5. 6. 7. 8.
Let this mixture until 50°C until 50°C Add NaOH solution Stir it Add 12 grams of alcohol alcohol Add 4 grams of glycerin glycerin Heat and stir it until clear clear
10 grams of coconut oil 1.Add 1 gram of 2.Heat until 70°C until stearic acid melts Brownish mixture 3. Let this mixture 4. Add NaOH solution 5.Stir it 6.Add 12 grams of alcohol 7. Add 4 grams of glycerin 8. Heat and stir it until clear
Clear Solution 9.
Let this mixture become cooler
10.
Add 1 mL of olive oil,dye, and Parfume
11.
Pour into the mold
Soap
10 grams of bulk oil 1.Add 1 gram of stearic acid 2. Heat until 70°C until all of stearic acid Brownish mixture 3.Let this mixture until 50°C 4. Add NaOH solution 5. Stir it 6. Add 12 grams of alcohol 7. Add 4 grams of glycerin 8. Heat and stir it until clear Clear solution 9. Let this mixture become cooler 10. Add 1 mL olive oil, dye and parfume 11. pour into the mold Soap
Clear Solution 9. Let this mixture become cooler 10. Add 1 mL olive oil, dye and parfume 11. Pour into the mold Soap
2. Emulsion Properties Of Soap 3 mL aquades 1. Added 5 drops oil 2. Added 2 mL soap solution (0,1-0,2 gr soap which di Ssolved in 6-8 mL of not water) 3. Shake it strongly 4. Observed the separation 5. Record the time Emulsion of soap
3 mL aquades 1. 2. 3. 4. 5.
Added 5 drops oil Shake it strongly Observed the separation Wait a minute Record the time
Emulsion
3 mL aquades 5. Added 5 drops oil 6. Added 2 mL soap solution (0,1-0,2 gr soap which di Ssolved in 6-8 mL of not water) 7. Shake it strongly 8. Observed the separation 9. Record the time
3 mL aquades 1. Added 5 drops oil 2. Added 2 mL soap solution (0,1-0,2 gr soap which di Ssolved in 6-8 mL of not water) 3. Shake it strongly 4. Observed the separation 5. Record the time
Emulsion of soap
Emulsion of soap
3 mL aquades
3 mL aquades
1. 2. 3.
1.Added 5 drops oil 2. Shake it strongly 3. Observed the separation 4. Wait a minute 5. Record the time
4. 5.
Added 5 drops oil Shake it strongly Observed the separation Wait a minute Record the time
Emulsion
Emulsion
3. Acid Number 5 grams of palm oil 1. Added 25 mL ethanol 2. Added 5 drops of PP indicator 3. Titration with KOH 0,1N As a standart solution Volume KOH 4.
Counted the number Of acid
Acid Number
5 grams of coconut oil 1. Added 25 mL ethanol 2. Added 5 drops of PP indicator 3. Titration with KOH 0,1N As a standart solution
Volume KOH 4.counted the number Of acid Acid Number
5 grams of bulk oil 1.
Added 25 mL ethanol 2. Added 5 drops of PP indicator 3. Titration with KOH 0,1N As a standart solution
Volume KOH 4.countedthe Of acid Acid Number
4. Saponification Number 1,5-2 grams of Palm oil 1. Entered into Erlenmeyer flask 2. Added 25 mL KOH alcoholic 0,5N 3. Refluxed for 30 minutes 4. Cooled and add 5 drops PP indicator 5. Titration with HCl solution 0,5N 6. Counted the saponification number Saponification Number
1,5-2 grams of coconut oil
1,5-2 grams of bulk oil
1. Entered into Erlenmeyer flask
1.Entered into Erlenmeyer flask
2. Added 25 mL KOH alcoholic
2. Added 25 mL KOH alcoholic
0,5N
0,5N
3. Refluxed for 30 minutes
3. Refluxed for 30 minutes
4. Cooled and add 5 drops PP
4. Cooled and add 5 drops PP indicator
indicator 5. Titration with HCl solution
5. Titration with HCl solution 0,5N
0,5N 6.
Counted the saponification number
Saponification Number
6.
Counted the saponification number
Saponification Number
1 piece
2. Spatula
1 piece
3. Pipette
10 piece
4. Stirring Rod
1 piece
5. Reflux condenser
1 piece
6. Funnel
1 piece
7. Separate Funnel
1 piece
8. Measuring glass
1 piece
9. Rounded bottom flask
1 piece
10. Erlenmeyer
1 piece
11. Clamps and statif
1 piece
12. Stem stirrer
1 piece
13. Filter paper
1 piece
14. Distillation condenser
1 piece
15. Thermometer
1 piece
16. Buret
1 piece
17. Ohaus balance sheet
1 piece
18. Tripod
1 piece
19. Rack
1 piece
20. Bunsen
1 piece
b. Materials 1. Coconut oil
22 grams
2. palm oil
22 gram
3. Bulk oil
22 grams
4. Ethanol
12 gram
5. NaOH
4.2 grams
6. Glycerin
12 grams
7. Olive oil
3 mL
8. Indicator PP
9 drops
9. Stearic acid
3 gram
10. Alcoholic KOH solution 0.1N
75 mL
11. Standard solution of 0.5 N HCl
30 mL
12. Dye
until enough
13. perfume
until enough
14. Aquades
until enough
G. LINES WORK 1. Soap Making 1,4 grams of NaOH 1. Disolved in 3,3 mL of water 2. Let it cool
NaOH solution
10 grams of Palm oil Add 1 gram of stearic acid stearic acid 2. Heat until 70°C until all all of of stearic acid melts 1.
Brownish mixture 3. 4. 5. 6. 7. 8.
Let this mixture until 50°C until 50°C Add NaOH solution Stir it Add 12 grams of alcohol alcohol Add 4 grams of glycerin glycerin Heat and stir it until clear clear
10 grams of coconut oil 1.Add 1 gram of 2.Heat until 70°C until stearic acid melts Brownish mixture 3. Let this mixture 4. Add NaOH solution 5.Stir it 6.Add 12 grams of alcohol 7. Add 4 grams of glycerin 8. Heat and stir it until clear
Clear Solution 9.
Let this mixture become cooler
10.
Add 1 mL of olive oil,dye, and Parfume
11.
Pour into the mold
Soap
10 grams of bulk oil 1.Add 1 gram of stearic acid 2. Heat until 70°C until all of stearic acid Brownish mixture 3.Let this mixture until 50°C 4. Add NaOH solution 5. Stir it 6. Add 12 grams of alcohol 7. Add 4 grams of glycerin 8. Heat and stir it until clear Clear solution 9. Let this mixture become cooler 10. Add 1 mL olive oil, dye and parfume 11. pour into the mold Soap
Clear Solution 9. Let this mixture become cooler 10. Add 1 mL olive oil, dye and parfume 11. Pour into the mold Soap
2. Emulsion Properties Of Soap 3 mL aquades 1. Added 5 drops oil 2. Added 2 mL soap solution (0,1-0,2 gr soap which di Ssolved in 6-8 mL of not water) 3. Shake it strongly 4. Observed the separation 5. Record the time Emulsion of soap
3 mL aquades 1. 2. 3. 4. 5.
Added 5 drops oil Shake it strongly Observed the separation Wait a minute Record the time
Emulsion
3 mL aquades 5. Added 5 drops oil 6. Added 2 mL soap solution (0,1-0,2 gr soap which di Ssolved in 6-8 mL of not water) 7. Shake it strongly 8. Observed the separation 9. Record the time
3 mL aquades 1. Added 5 drops oil 2. Added 2 mL soap solution (0,1-0,2 gr soap which di Ssolved in 6-8 mL of not water) 3. Shake it strongly 4. Observed the separation 5. Record the time
Emulsion of soap
Emulsion of soap
3 mL aquades
3 mL aquades
1. 2. 3.
1.Added 5 drops oil 2. Shake it strongly 3. Observed the separation 4. Wait a minute 5. Record the time
4. 5.
Added 5 drops oil Shake it strongly Observed the separation Wait a minute Record the time
Emulsion
Emulsion
3. Acid Number 5 grams of palm oil 1. Added 25 mL ethanol 2. Added 5 drops of PP indicator 3. Titration with KOH 0,1N As a standart solution Volume KOH 4.
Counted the number Of acid
Acid Number
5 grams of coconut oil 1. Added 25 mL ethanol 2. Added 5 drops of PP indicator 3. Titration with KOH 0,1N As a standart solution
Volume KOH 4.counted the number Of acid Acid Number
5 grams of bulk oil 1.
Added 25 mL ethanol 2. Added 5 drops of PP indicator 3. Titration with KOH 0,1N As a standart solution
Volume KOH 4.countedthe Of acid Acid Number
4. Saponification Number 1,5-2 grams of Palm oil 1. Entered into Erlenmeyer flask 2. Added 25 mL KOH alcoholic 0,5N 3. Refluxed for 30 minutes 4. Cooled and add 5 drops PP indicator 5. Titration with HCl solution 0,5N 6. Counted the saponification number Saponification Number
1,5-2 grams of coconut oil
1,5-2 grams of bulk oil
1. Entered into Erlenmeyer flask
1.Entered into Erlenmeyer flask
2. Added 25 mL KOH alcoholic
2. Added 25 mL KOH alcoholic
0,5N
0,5N
3. Refluxed for 30 minutes
3. Refluxed for 30 minutes
4. Cooled and add 5 drops PP
4. Cooled and add 5 drops PP indicator
indicator 5. Titration with HCl solution
5. Titration with HCl solution 0,5N
0,5N 6.
Counted the saponification number
Saponification Number
6.
Counted the saponification number
Saponification Number
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